Related two-pulse MQ-MAS references
Below are provided some NMR references about MQ-MAS with two-pulse sequence
applied to half-integer quadrupole spins. These references contain
(1) the pulse-sequence diagram,
(2) the coherence-transfer pathways,
(3) the phase-cycling.
-
D. Massiot, F. Fayon, M. Capron, I. King, S. Le Calvé, B. Alonso,
J.-O. Durand, B. Bujoli, Z. Gan, and G. Hoatson
Modelling one- and two-dimensional solid-state NMR spectra,
Magn. Reson. Chem. 40, 70-76 (2002). -
M. Bak, J. T. Rasmussen, and N. C. Nielsen
SIMPSON: A general simulation program for solid-state NMR spectroscopy, (1)
J. Magn. Reson. 147, 296-330 (2000). -
C. Bonhomme and J. Livage
Pictorial representation of anisotropy and macroscopic reorientations of samples in solid-state NMR: Second-order interactions,
J. Phys. Chem. A 103, 460-477 (1999). -
J. McManus, R. Kemp-Harper, and S. Wimperis
Second-order quadrupolar-dipolar broadening in two-dimensional MQMAS NMR,
Chem. Phys. Lett. 311, 292-298 (1999). -
J.-P. Amoureux and C. Fernandez
Triple, quintuple and higher order multiple quantum MAS NMR of quadrupolar nuclei,
Solid State Nucl. Magn. Reson. 10, 211-223 (1998).
Erratum: Solid State Nucl. Magn. Reson. 16, 339-343 (2000). -
L. Marinelli, A. Medek, and L. Frydman
Composite pulse excitation schemes for MQMAS NMR of half-integer quadrupolar spins,
J. Magn. Reson. 132, 88-95 (1998). -
S. Ding and C. A. McDowell
MQ-MAS NMR spectroscopy of spin-3/2 quadrupolar spin systems using shaped pulses,
J. Magn. Reson. 135, 61-69 (1998). -
S. Ding and C. A. McDowell
Shaped pulse excitation in MQ MAS spectroscopy of half-integer quadrupole spin systems,
Chem. Phys. Lett. 270, 81-86 (1997). -
P. P. Man
Second-order quadrupole effects on Hahn echoes in fast-rotating solids at the magic angle (PDF article, 320 Kb),
Phys. Rev. B 55, 8406-8424 (1997). -
L. Marinelli and L. Frydman
On the origin of spinning sidebands in MQMAS NMR,
Chem. Phys. Lett. 275, 188-198 (1997). -
D. Massiot
Sensitivity and lineshape improvements of MQ-MAS by rotor-synchronized data acquisition,
J. Magn. Reson. A 122, 240-244 (1996). -
J.-P. Amoureux, C. Fernandez, and L. Frydman
Optimized MQ MAS NMR experiments on half-integer quadrupoles,
Chem. Phys. Lett. 259, 347-355 (1996). -
A. Samoson
2D isotropic NMR of quadrupole nuclei in solids,
J. Magn. Reson. A 121, 209-211 (1996). -
C. Jäger, K. Herzog, B. Thomas, M. Feike, and G. Kunath-Fandrei
Detection of multiple boron sites in glasses by 11B satellite transition nuclear magnetic resonance spectroscopy, (1)(2)
Solid State Nucl. Magn. Reson. 5, 51-61 (1995). -
A. Samoson
Multiquantum NMR of quadrupole nuclei with strong pulses, (1)(3)
Chem. Phys. Lett. 247, 203-206 (1995). -
J.-P. Amoureux
High-resolution solid-state NMR for spin 3/2 and 9/2: the multi-quantum transition method,
Solid State Nucl. Magn. Reson. 2, 83-88 (1993).