CP-MAS

Some NMR references about CP-MAS pulse sequences applied to half-integer quadrupole spins:

1. S. P. Puls and H. Eckert
   Site discrimination in mixed-alkali glasses studied by cross-polarization NMR,
   J. Phys. Chem. B 110, 14253-14261 (2006).
2. M. Edén
   Quadrupolar coupling selective cross-polarization in solid state NMR,
   Phys. Chem. Chem. Phys. 8, 1994-1999 (2006).
3. Gregor Mali and Venceslav Kaucic
   Determination of distances between aluminum and spin-1/2 nuclei using cross polarization with very weak radio-frequency fields,
   J. Chem. Phys. 117, 3327-3339 (2002).
4. G. Mali, A. Meden, A. Ristic, N. N. Tusar, and V. Kaucic
   Interaction of dipropylamine template molecules with the framework of as-synthesized AlPO₄-31,
   J. Phys. Chem. B 106, 63-69 (2002).
5. J.-P. Amoureux and M. Pruski
   Theoretical and experimental assessment of single- and multiple-quantum cross-polarization in solid state NMR,
   Mol. Phys. 100, 1595-1613 (2002).
6. S. E. Ashbrook and S. Wimperis
   Single- and multiple-quantum cross-polarization in NMR of quadrupolar nuclei in static samples,
   Mol. Phys. 98, 1-26 (2000).
7. J. M. Egan, R. M. Wenslow, and K. T. Mueller
   Mapping aluminum/phosphorus connectivities in aluminophosphate glasses,
   J. Non-Cryst. Solids 261, 115-126 (2000).
8. M. A. Eastman
   Examples of Hartmann-Hahn match conditions for CP/MAS between two half-integer quadrupolar nuclei,
   J. Magn. Reson. 139, 98-108 (1999).
9. S. Ding and C. A. McDowell
   Application of Floquet theory to quadrupolar nuclear spin-5/2 nuclei in solids undergoing sample rotation,
   Mol. Phys. 95, 841-848 (1998).
10. M. Tomaselli, D. deGraw, J. L. Yarger, M. P. Augustine, and A. Pines
    Scalar and anisotropic J interactions in undoped InP: a triple-resonance NMR study,
    Phys. Rev. B 58, 8627-8633 (1998).
11. Jerry C. C. Chan, Marko Bertmer, and Hellmut Eckert
    Double-quantum cross-polarization between half-integer quadrupolar spin systems: ¹¹B <-> ²³Na and ¹¹B <-> ²⁷Al,
    Chem. Phys. Lett. 292, 154-160 (1998).
12. E. R. H. van Eck and M. E. Smith
    Orientation of the quadrupole and dipole tensors of hydroxyl groups by ¹⁷O quadrupole separated local field NMR,
    J. Chem. Phys. 108, 5904-5912 (1998).
13. S. M. De Paul, M. Ernst, J. S. Shore, J. F. Stebbins, and A. Pines
    Cross-polarization from quadrupolar nuclei to silicon using low-radio-frequency amplitudes during MAS,
    J. Phys. Chem. B 101, 3240-3249 (1997).
14. L. van Wüllen, L. Züchner, W. Müller-Warmuth, and H. Eckert
    ¹¹B{²⁷Al} and ²⁷Al{¹¹B} double resonance experiments on a glassy sodium aluminoborate,
    Solid State Nucl. Magn. Reson. 6, 203-212 (1996).
15. G. G. Almond, R. K. Harris, and K. R. Franklin
    ¹H, ²⁹Si and ¹H, ²³Na heteronuclear shift correlation in octosilicate via cross-polarisation,
    Solid State Nucl. Magn. Reson. 6, 31-38 (1996).
16. T. P. Jarvie, R. M. Wenslow, and K. T. Mueller
    High-resolution solid-state heteronuclear correlation NMR for quadrupolar and spin-1/2 nuclei,
    J. Am. Chem. Soc. 117, 570-571 (1995).
17. S. Ding and C. A. McDowell
    Theoretical calculations of the CPMAS spectral lineshapes of half-integer quadrupole systems,
    J. Magn. Reson. A 114, 80-87 (1995).
18. P. J. Barrie
    Distorted powder lineshapes in ²⁷Al CP/MAS NMR spectroscopy of solids,
    Chem. Phys. Lett. 208, 486-490 (1993).
19. S. Hayashi and K. Hayamizu
    Errata: Line shapes in CP/MAS NMR spectra of half-integer quadrupolar nuclei,
    Chem. Phys. Lett. 205, 597-597 (1993).
20. S. Hayashi and K. Hayamizu
    Line shapes in CP/MAS NMR spectra of half-integer quadrupolar nuclei,
    Chem. Phys. Lett. 203, 319-324 (1993).
21. C. A. Fyfe, K. T. Mueller, H. Grondey, and K. C. Wong-Moon
    Solid-state double-resonance NMR experiments involving quadrupolar and spin 1/2 nuclei,
    J. Phys. Chem. 97, 13484-13495 (1993).
22. C. A. Fyfe, H. Grondey, K. T. Mueller, K. C. Wong-Moon, and T. Markus
    Coherence transfer involving quadrupolar nuclei in solids: ²⁷Al<->³¹P cross-polarization NMR in the molecular sieves VPI-5,
    J. Am. Chem. Soc. 114, 5876-5878 (1992).
23. A. J. Vega
    CP/MAS of quadrupolar S = 3/2 nuclei,
    Solid State Nucl. Magn. Reson. 1, 17-32 (1992).
24. R. K. Harris and G. J. Nesbitt
    Cross polarization for quadrupolar nuclei---Proton to sodium-23,
    J. Magn. Reson. 78, 245-256 (1988).

Related bibliography

1. Sean C. Christiansen, Niklas Hedin, Jan D. Epping, Michael T. Janicke, Yolanda del Amo, Mark Demarest, Mark Brzezinski, and Bradley F. Chmelka
   Sensitivity considerations in polarization transfer and filtering using dipole–dipole couplings: Implications for biomineral systems,
   Solid State Nucl. Magn. Reson. 29, 170-182 (2006).
   Abstract
2. M. Ernst-M, H. Geen, and B. H. Meier
   Amplitude-modulated decoupling in rotating solids: A bimodal Floquet approach,
   Solid State Nucl. Magn. Reson. 29, 2-21 (2006).
3. K. Gopalakrishnan and G. Bodenhausen
   Cross polarization from spins I = 1/2 to spins S = 1 in nuclear magnetic resonance with magic angle sample spinning,
   J. Chem. Phys. 124, 194311/1-194311/14 (2006).
4. S. V. Dvinskikh and V. I. Chizhik
   Cross-polarization with radio-frequency field phase and amplitude modulation under magic-angle spinning conditions,
   J. Exp. Theo. Phys. 102, 91-101 (2006).
5. C. Lejeune, C. Coelho, L. Bonhomme-Coury, T. Azaïs, J. Maquet, and C. Bonhomme
   Studies of silicophosphate derivatives by ³¹P -> ²⁹Si CP MAS NMR,
   Solid State Nucl. Magn. Reson. 27, 242-246 (2005).
6. Robert E. Taylor
   ¹³C CP/MAS: Application to glycine,
   Concepts Magn. Reson. A 22, 79-89 (2004).
7. Robert E. Taylor
   Setting up ¹³C CP/MAS experiments,
   Concepts Magn. Reson. A 22, 37-49 (2004).
8. H. Kampermann, A. D. Bain, and R. S. Dumont
   Residual dipolar coupling in the CP/MAS nuclear magnetic resonance spectra of spin-1/2 nuclei coupled to quadrupolar nuclei application of floquet theory,
   J. Chem. Phys. 116, 2464-2471 (2002).
9. G. Metz, X. Wu, and S. O. Smith
   Ramped-amplitude cross polarization in magic-angle-spinning NMR,
   J. Magn. Reson. A 110, 219-227 (1994).
10. B. H. Meier
    Cross polarization under fast magic angle spinning: thermodynamical considerations,
    Chem. Phys. Lett. 188, 201-207 (1992).
11. E. O. Stejskal and J. Schaefer
    Removal of artifacts from cross-polarization NMR experiments,
    J. Magn. Reson. 18, 560-563 (1975).
12. A. Pines, M. G. Gibby, and J. S. Waugh
    Proton-enhanced NMR of dilute spins in solids,
    J. Chem. Phys. 59, 569-590 (1973).
13. S. R. Hartmann and E. L. Hahn
    Nuclear double resonance in the rotating frame,
    Phys. Rev. 128, 2042-2053 (1962).