Zinc-67 NMR

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Isotope Spin Natural
abundance (%)
Quadrupole moment
NMR frequency (MHz)
at a field of 2.3488T
Zn-67 5/2 4.11 15.0 2.85E-3 1.17E-4 -6.254 Zn(NO3)2

Solid-state zinc NMR references

  1. Rasmus S. K. Madsen, Ang Qiao, Jishnu Sen, Ivan Hung, Kuizhi Chen, Zhehong Gan, Sabysachi Sen, and Yuanzheng Yue
    Ultrahigh-field 67Zn NMR reveals short-range disorder in zeolitic imidazolate framework glasses,
    Science 367, 1473-1476 (2020).
  2. Yining Huang and Andre Sutrisno
    Recent advances in solid-state 67Zn NMR studies: from nanoparticles to biological systems,
    Annu. Rep. Nucl. Magn. Reson. Spectrosc. 81, 1-46 (2014).
  3. Léo Choubrac, Michaël Paris, Alain Lafond, Catherine Guillot-Deudon, Xavier Rocquefelte, and Stéphane Jobic
    Multinuclear (67Zn, 119Sn and 65Cu) NMR spectroscopy – an ideal technique to probe the cationic ordering in Cu2ZnSnS4 photovoltaic materials,
    Phys. Chem. Chem. Phys. 15, 10722-10725 (2013).
  4. Xingyu Lu, Olivier Lafon, Julien Trébosc, and Jean-Paul Amoureux
    Detailed analysis of the S-RESPDOR solid-state NMR method for inter-nuclear distance measurement between spin-1/2 and quadrupolar nuclei,
    J. Magn. Reson. 215, 34-49 (2012).
  5. Andre Sutrisno, Li Liu, Jun Xu, and Yining Huang
    Natural abundance solid-state 67Zn NMR characterization of microporous zinc phosphites and zinc phosphates at ultrahigh magnetic field,
    Phys. Chem. Chem. Phys 13, 16606-16617 (2011).
  6. T. J. Bastow and S. Celotto
    25Mg NMR site analysis in metals and intermetallics,
    Solid State Nucl. Magn. Reson. 35, 217-222 (2009).
  7. A. S. Lipton, M. M. Morlok, G. Parkin, and P. D. Ellis
    67Zn solid-state NMR spectroscopy of {[TpBut,Me)]Zn(OH2)}[HOB(C6F5)3]. The importance of the anion [HOB(C6F5)3]-,
    Inorg. Chem. 47, 5184-5189 (2008).
  8. Y. Zhang, S. Mukherjee, and E. Oldfield
    67Zn NMR chemical shifts and electric field gradients in zinc complexes: A quantum chemical investigation,
    J. Am. Chem. Soc. 127, 2370-2371 (2005).
  9. F. H. Larsen
    Molecular dynamics of half-integer quadrupolar nuclei studied by QCPMG solid-state NMR experiments on static and rotating samples. Theory and simulations,
    J. Magn. Reson. 171, 293-304 (2004).
  10. A. S. Lipton, R. W. Heck, J. A. Sears, and P. D. Ellis
    Low temperature solid-state NMR experiments of half-integer quadrupolar nuclides: caveats and data analysis,
    J. Magn. Reson. 168, 66-74 (2004).
  11. T. J. Bastow
    67Zn NMR investigation of zinc halides,
    Chem. Phys. Lett. 380, 516-520 (2003).
  12. A. S. Lipton, T. A. Wright, M. K. Bowman, D. L. Reger, and P. D. Ellis
    Solid-state 67Zn NMR spectroscopy in bioinorganic chemistry. Spectra of four- and six-coordinate zinc pyrazolylborate complexes obtained by management of proton relaxation rates with a paramagnetic dopant,
    J. Am. Chem. Soc. 124, 5850-5860 (2002).
  13. F. H. Larsen, J. Skibsted, H. J. Jakobsen, and N. C. Nielsen
    Solid-state QCPMG NMR of low-gamma quadrupolar metal nuclei in natural abundance,
    J. Am. Chem. Soc. 122, 7080-7086 (2000).
  14. G. Wu
    Zinc-67 NMR spectroscopy of solids,
    Chem. Phys. Lett. 298, 375-380 (1998).
  15. Gang Wu
    Recent developments in solid-state nuclear magnetic resonance of quadrupolar nuclei and applications to biological systems,
    Biochem. Cell Biol. 76, 429-442 (1998).
  16. T. J. Bastow
    67Zn NMR in zinc metal,
    J. Phys.: Condens. Matter 8, 11309-11315 (1996).
  17. S. F. Dec, M. F. Davis, G. E. Maciel, C. E. Bronnimann, J. J. Fitzgerald, and S. S. Han
    Solid-state multinuclear NMR studies of ferroelectric, piezoelectric, and related materials,
    Inorg. Chem. 32, 955-959 (1993).
  18. A. C. Kunwar, G. L. Turner, and E. Oldfield
    Solid-state spin-echo Fourier transform NMR of 39K and 67Zn salts at high field,
    J. Magn. Reson. 69, 124-127 (1986).

More solid-state Zn-67 NMR references.

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