Amplitude-modulated MQMAS experiments:

• Z-filter
  The same pulse program as that defined for XWINNMR 3.5 operating system
• SPAM-echo/antiecho (2D only)
  The only change is the addtion of 3u delay before the two signal storage lines in the pulse program for XWINNMR 3.5 operating system
• MQMAS data processing:
  Shearing the 2D spectrum with AU program xfshear
• Bruker NMR Manual for MQMAS Experiment:
  Manual created by: IMSERC Lab, Department of Chemistry, Northwestern University
  Manual revised date: November 2019
• ssNMRlib: a comprehensive library and tool box for acquisition of solid-state nuclear magnetic resonance experiments on Bruker spectrometers
  Magn. Reson. 1, 331–345 (2020).
  Open access
• Akiko Sasaki, Yu Tsutsumi, Jean-Paul Amoureux
  Accelerating high-resolution NMR of half-integer quadrupolar nuclei in solids: SPAM-MQMAS and SPAM-STMAS,
  Solid State Nucl. Magn. Reson. 108, 101668/1-101668/14 (2020).
  Abstract

• z-filter ±3QMAS for I = 3/2, 5/2, and 7/2
• z-filter ±5QMAS for I = 5/2, 7/2, and 9/2
• z-filter ±7QMAS for I = 7/2 and 9/2
• z-filter ±9QMAS for I = 9/2

Phase-modulated MQMAS experiments:

• Multiplex SPAM (2D only)
  The same pulse program as that defined for XWINNMR 3.5 operating system
• The AU program MSM (Multiplex SPAM MQ) remains valid

1. Advanced Quadrupolar NMR (6 Mb PDF file) by Sharon Ashbrook, School of Chemistry, University of St Andrews
2. High-resolution solid-state NMR of quadrupolar nuclei, tutorial lecture presented at the Bruker user's meeting Breckenridge, Colorado July 2007 (25 Mb PDF file) by Philip J. Grandinetti, Ohio State University
3. Applications of nuclear magnetic resonance to metal hydrogen materials, Summer School Lectures presented at MH2008 23 June 2008 (5 Mb PDF file) by Son-Jong Hwang and Robert C. Bowman, Jr. California Institute of Technology, Pasadena
4. High-field solid-state NMR: The tools and their application in materials research, Lectures presented at the International School on "MAGNETIC FIELDS FOR SCIENCE", Cargèse, Corsica, France, August 27th - September 8th, 2007 (10 Mb PDF file) by Arno Kentgens Department of Physical Chemistry / solid-state NMR, Institute for Molecules and Materials, Radboud University Nijmegen, The Netherlands