2Q/1Q correlation with DUMBO decoupling experiments:

cnst31: sample rotation frequency

t1 increment: inf1 = X and -X windowed DUMBO cycle duration = p25 = 2*l3*(2*d3+p20)

-----------------------------

• B1=7*cnst31
• DUMBOdqPC7sqbsw1d: 1D big F1 spectral width PC7 2Q/1Q correlation.
• DUMBOdqPC7sqbsw: 2D pulse program.
  ----------------------------
• B1=7*cnst31
• DUMBOdqR1426sqbsw1d: 1D big F1 spectral width R14_2^6 2Q/1Q correlation.
• DUMBOdqR1426sqbsw: 2D pulse program.
  ----------------------------
• B1=5*cnst31
• DUMBOdqSPC5sqbsw1d: 1D big F1 spectral width SPC5 2Q/1Q correlation.
• DUMBOdqSPC5sqbsw: 2D pulse program.
  
• DUMBOdqSPC5sq: 2D pulse program (non big F1 spectral width).
  ----------------------------
• B1=3*cnst31
• DUMBOdqR1225sqbsw1d: 1D big F1 spectral width R12_2^5 2Q/1Q correlation.
• DUMBOdqR1225sqbsw: 2D pulse program.
  ----------------------------
• B1=1.75*cnst31
• DUMBOdqR1445sqbsw1d: 1D big F1 spectral width R14_4^5 2Q/1Q correlation.
• DUMBOdqR1445sqbsw: 2D pulse program.
• DUMBOdqR1445sq: 2D pulse program (non big F1 spectral width).
  ----------------------------
• B1 and cnst31 are independent
• DUMBOdqBABA1sq1d: 1D homonuclear BABA1 2Q/1Q correlation.
  
• DUMBOdqBABA1sq: 2D homonuclear BABA1 2Q/1Q correlation.
  

1. Tutorial (PDF file, 9 Mb) on "Heteronuclear spin decoupling in magic-angle-spinning solid-state NMR", by Matthias Ernst, ETH Zürich, 2008.
2. Tutorial (PDF file, 3 Mb) on "Manipulating the Hamiltonian: decoupling and recoupling", by Jeremy Titman, School of Chemistry, University of Nottingham.
3. Tutorial (PDF file, 4 Mb) on "Numerical methods for pulse sequence optimisation", by Lyndon Emsley, Laboratoire de Chimie, Ecole Normale Supérieure de Lyon, and Institut Universitaire de France.
4. Varian user meeting, Taichung, June 13, 2006 (PDF file, 7 Mb) on "Some recent progress of solid state NMR spectroscopy (and micro-imaging): methods and applications", by Shangwu Ding, Department of Chemistry, National Sun Yat-sen University.
5. Second winterschool on biomolecular solid-state, Stowe Vermont, January 24-29, 2010 (PDF file, 3 Mb) on "Floquet theory in solid state NMR, theory and applications, homonuclear decoupling", by Shimon Vega with Michal Leskes and P. K. Madhu, Weizmann Institute of Science.
6. Tutorial (PDF file, 5 Mb) on "Two-dimensional correlation spectroscopy in solids", by Jeremy Titman, School of Chemistry, University of Nottingham.