Zirconium-91 NMR
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Isotope Spin Natural
abundance (%)		 Quadrupole moment
(10-30m2)		 Relative
sensitivity		 Absolute
sensitivity		 NMR frequency (MHz)
at a field of 2.3488T		 Reference
sample
Zr-91 5/2 11.23 -17.6 9.48E-3 1.06E-3 9.330 Zr(C5H5)2Cl2

Solid-state zirconium NMR references

  1. Jiří Czernek, Libor Kobera, Lubomír Havlák, Vladimíra Czerneková, Jan Rohlíček, Jan Bárta, and Jiří Brus
    Probing the 91Zr NMR parameters in the solid state by a combination of DFT calculations and experiments,
    Chem. Phys. Lett. 738, 136855-136859 (2020).
    Abstract
  2. Bryan E.G. Lucier and Yining Huang
    A review of 91Zr solid-state nuclear magnetic resonance spectroscopy,
    Annu. Rep. Nucl. Magn. Reson. Spectrosc. 84, 233-289 (2015).
    Abstract
  3. Andre Sutrisno, Lei Liu, Jinxiang Dong, and Yining Huang
    Solid-state 91Zr NMR characterization of layered and three-dimensional framework zirconium phosphates,
    J. Phys. Chem. C 116, 17070-17081 (2012).
    Abstract
  4. A. J. Rossini, I. Hung, S. A. Johnson, C. Slebodnick, M. Mensch, P. A. Deck, and R. W. Schurko
    Solid-state 91Zr NMR spectroscopy studies of zirconocene olefin polymerization catalyst precursors,
    J. Am. Chem. Soc. 132, 18301-18317 (2010).
    Abstract
  5. Sharon E. Ashbrook
    Recent advances in solid-state NMR spectroscopy of quadrupolar nuclei,
    Phys. Chem. Chem. Phys. 11, 6892-6905 (2009).
    Abstract
  6. O. Pauvert, F. Fayon, A. Rakhmatullin, S. Kramer, M. Horvati, D. Avignant, C. Berthier, M. Deschamps, D. Massiot, and C. Bessada
    91Zr nuclear magnetic resonance spectroscopy of solid zirconium halides at high magnetic field,
    Inorg. Chem. 48, 8709-8717 (2009).
    Abstract
  7. Joel A. Tang, Luke A. O’Dell, Pedro M. Aguiar, Bryan E. G. Lucier, Dimitris Sakellariou, and Robert W. Schurko
    Application of static microcoils and WURST pulses for solid-state ultra-wideline NMR spectroscopy of quadrupolar nuclei ,
    Chem. Phys. Lett. 466, 227-234 (2008).
    Abstract
  8. Luke A. O’Dell and Robert W. Schurko
    QCPMG using adiabatic pulses for faster acquisition of ultra-wideline NMR spectra,
    Chem. Phys. Lett. 464, 97-102 (2008).
    Abstract
  9. J. F. Zhu, Z. Lin, Z. M. Yan, and Y. N. Huang
    91Zr and 25Mg solid-state NMR characterization of the local environments of the metal centers in microporous materials,
    Chem. Phys. Lett. 461, 260-265 (2008).
  10. I. Hung and R.W. Schurko
    Solid-state 91Zr NMR of bis(cyclopentadienyl)dichloro zirconium(IV),
    J. Phys. Chem. B 108, 9060-9069 (2004).
  11. M. E. Smith and E. R. H. van Eck
    Recent advances in experimental solid state NMR methodology for half-integer spin quadrupolar nuclei,
    Prog. Nucl. Magn. Reson. Spectrosc. 34, 159-201 (1999).
  12. S. F. Dec, M. F. Davis, G. E. Maciel, C. E. Bronnimann, J. J. Fitzgerald, and S. S. Han
    Solid-state multinuclear NMR studies of ferroelectric, piezoelectric, and related materials,
    Inorg. Chem. 32, 955-959 (1993).
  13. T. J. Bastow, M. E. Smith, and S. N. Stuart
    Observation of 91Zr NMR in zirconium-based metals and oxides,
    Chem. Phys. Lett. 191, 125-129 (1992).
  14. T. J. Bastow and M. E. Smith
    91Zr NMR characterisation of phases in transformation toughened zirconia,
    Solid State Nucl. Magn. Reson. 1, 165-174 (1992).
  15. J. S. Hartman, F. P. Koffyberg, and J. A. Ripmeester
    An exploration of 91Zr solid-state NMR of synthetic oxide materials,
    J. Magn. Reson. 91, 400-404 (1991).

Related bibliography

  1. Sylvia M. Draper and Brendan Twamley
    Zirconium 1992,
    Coord. Chem. Rev. 146, A91-A140 (1995).
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