Aluminum-27 NMR

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Isotope Spin Natural
abundance (%)
Quadrupole moment
NMR frequency (MHz)
at 2.3488T
Al-27 5/2 100 14.66 0.21 0.21 -26.057 Al(NO3)3

Directory of solid-state Al-27 NMR references
Single Crystal (單晶) Crystalline Powder (晶型粉末)
Alpha-, Gamma-Al2O3, Micro-Porous, Mineral...
Amorphous Powder (非晶型粉末)

Solid-state aluminum NMR references

  1. Bodo Zibrowius and Michael Fischer
    On the use of Solomon echoes in 27Al NMR studies of complex aluminium hydrides,
    ChemistryOpen, e202300011/1-e202300011/9 (2023).
    Open access
  2. Lara Sulcek, Bernd Marler, and Michael Fechtelkord
    Cation and anion ordering in synthetic lepidolites and lithian muscovites: influence of the OH/F and Li/Al ratios on the mica formation studied by NMR (nuclear magnetic resonance) spectroscopy and X-ray diffraction,
    Eur. J. Mineral. 35, 199-217 (2023).
    Open Access
  3. Libor Kobera, Jiri Dedecek, Petr Klein, Edyta Tabor, Jiri Brus, Anna V. Fishchuk, and Stepan Sklenak
    Formation and local structure of framework Al Lewis sites in beta zeolites,
    J. Chem. Phys. 156, 104702-1-104702-12 (2022).
  4. Konstantin Khivantsev, Nicholas R. Jaegers, Libor Kovarik, Miroslaw A. Derewinski, Ja-Hun Kwak, and Janos Szanyi
    On the nature of extra-framework aluminum species and improved catalytic properties in steamed zeolites,
    Molecules 27, 2352/1-2352/12 (2022).
    Open access
  5. Thomas M. Osborn Popp, Nicholas H. Alaniva, and Alexander B. Barnes
    Setting the magic angle using single crystal sapphire rotors,
    J. Magn. Reson. Open 8-9, 100019/1-100019/7 (2021).
    Open access
  6. Andrii Mahun, Sabina Abbrent, Jiri Czernek, Jan Rohlicek, Hana Macková, Weihua Ning, Rafał Konefał, Jiří Brus, and Libor Kobera
    Reconstructing reliable powder patterns from spikelets (Q)CPMG NMR spectra: Simplification of UWNMR crystallography analysis,
    Molecules 26, 6051/1-6051/13 (2021).
    Open access
  7. Marianna Porcino, Xue Li, Ruxandra Gref, and Charlotte Martineau-corcos
    Solid state NMR spectroscopy as a powerful tool to investigate the location of fluorinated lipids in highly porous hybrid organic-inorganic nanoparticles,
    Magn. Reson. Chem. 59, 1038-1047 (2021).
  8. Hiroki Nagashima, Julien Trébosc, Yoshihiro Kon, Olivier Lafon, and Jean-Paul Amoureux
    Efficient transfer of DNP-enhanced 1H magnetization to half-integer quadrupolar nuclei in solids at moderate spinning rate,
    Magn. Reson. Chem. 59, 920-939 (2021).
  9. Nghia Tuan Duong, Daniel Lee, Frédéric Mentink-Vigier, Olivier Lafon, and Gaël De Paëpe
    On the use of radio-frequency offsets for improving double quantum homonuclear dipolar recoupling of half-integer quadrupolar nuclei,
    Magn. Reson. Chem. 59, 991-1008 (2021).
  10. Mingji Zheng, Shaohui Xin, Qiang Wang, Julien Trébosc, Jun Xu, Guodong Qi, Ningdong Feng, Olivier Lafon, and Feng Deng
    Through-space 11B–27Al correlation: Influence of the recoupling channel,
    Magn. Reson. Chem. 59, 1062-1076 (2021).
  11. Callum Cross, Luca Cervini, Nathan R. Halcovitch, and John M. Griffin
    Solid-state nuclear magnetic resonance study of polymorphism in tris(8-hydroxyquinolinate)aluminium,
    Magn. Reson. Chem. 59, 1024-1037 (2021).
    Open access
  12. Kent J. Griffith, Fenghua Ding, and Steven Flynn
    Solid-state nuclear magnetic resonance of spin-9/2 nuclei 115In and 209Bi in functional inorganic complex oxides,
    Magn. Reson. Chem. 59, 1077-1088 (2021).
  13. Jennifer S. Gómez, Andrew G. M. Rankin, Julien Trébosc, Frédérique Pourpoint, Yu Tsutsumi, Hiroki Nagashima, Olivier Lafon, and Jean-Paul Amoureux
    Improved NMR transfer of magnetization from protons to half-integer spin quadrupolar nuclei at moderate and high magic-angle spinning frequencies,
    Magn. Reson. 2, 447-464 (2021).
  14. Pedro B. Groszewicz
    NMR spectroscopy of electroceramics – Applications to lead-free perovskite oxides,
    Open Ceram. 5, 100083/1-100083/17 (2021).
    Open access
  15. Luizianne P. Alves, Rosane A. S. San Gil, Arnaldo C. Faro Júnior, Leandro B. Borré, Stevie H. Lima, Helio R. X. Pimentel, and Angela S. Rocha
    Development and validation of an analytical methodology for quantification of Al in alumina-based materials by 27Al solid-state NMR,
    Int. J. Dev. Res. 11, 45249-45255 (2021).
    Open access
  16. Samuel J. Page, Angelo Gallo, Steven P. Brown, Józef R. Lewandowski, John V. Hanna, and W. Trent Franks
    Simultaneous MQMAS NMR experiments for two half-integer quadrupolar nuclei,
    J. Magn. Reson. 320, 106831/1-106831/7 (2020).
    Open access
  17. Marie Duffiet , Maxime Blangero, Pierre Etienne Cabelguen, Kyeong Se Song, François Fauth, Claude Delmas, and Dany Carlier
    Probing Al distribution in LiCo0.96Al0.04O2 materials using 7Li, 27Al, and 59Co MAS NMR combined with synchrotron X-ray diffraction,
    Inorg. Chem. 59, 2890-2899 (2020).
  18. Kent J. Griffith, Michael A. Hope, Philip J. Reeves, Mark Anayee, Yury Gogotsi, and Clare P. Grey
    Bulk and surface chemistry of the niobium MAX and MXene phases from multinuclear solid-state NMR spectroscopy,
    J. Am. Chem. Soc. 142, 18924-18935 (2020).
  19. Yang Yu, Philipp Keil, Michael Ryan Hansen, and Mattias Edén
    Improved magnetization transfers among quadrupolar nuclei in two-dimensional homonuclear correlation NMR experiments applied to inorganic network structures,
    Molecules 25, 337/1-337/23 (2020).
    Open access
  20. Mariusz Gackowski, Jerzy Podobiński, Ewa Broclawik, and Jerzy Datka
    IR and NMR studies of the status of Al and acid sites in desilicated zeolite Y,
    Molecules 25, 31/1-31/12 (2020).
    Open access
  21. Zichun Wang, Tong Li, Yijiao Jiang, Olivier Lafon, Zongwen Liu, Julien Trébosc, Alfons Baiker, Jean-Paul Amoureux, and Jun Huang
    Acidity enhancement through synergy of penta- and tetra-coordinated aluminum species in amorphous silica networks,
    Nat. Commun. 11, 225/1-225/9 (2020).
    Open access
  22. Otto E. O. Zeman, Igor L. Moudrakovski, Carsten Hartmann, Sylvio Indris, and Thomas Bräuniger
    Local electronic structure in AlN studied by single-crystal 27Al and 14N NMR and DFT calculations,
    Molecules 25, 469/1-469/13 (2020).
    Open access
  23. Xiaojing Jin, Yannick Millot, Céline Sayag, Juliette Blanchard, and Pascal P. Man
    Influence of dealumination by acetylacetone on acidity and activity of amorphous silica‐aluminas,
    ChemistrySelect 5, 2489-2495 (2020).
  24. Frédéric A. Perras, Zichun Wang, Takeshi Kobayashi, Alfons Baiker, Jun Huang, and Marek Pruski
    Shedding light on the atomic-scale structure of amorphous silica–alumina and its Brønsted acid sites,
    Phys. Chem. Chem. Phys. 21, 19529-19537 (2019).
  25. Andraž Mavrič, Matjaz Valant, Chunhua Cui, and Zhiming M. Wang
    Advanced applications of amorphous alumina: From nano to bulk,
    J. Non-Cryst. Solids 521, 119493-119493/15 (2019).
  26. Shaohui Xin, Qiang Wang, Jun Xu, Yueying Chu, Pengfei Wang, Ningdong Feng, Guodong Qi, Julien Trébosc, Olivier Lafon, Weibin Fan, and Feng Deng
    The acidic nature of “NMR-invisible” tricoordinated framework aluminum species in zeolites,
    Chem. Sci. 10, 10159-10169 (2019).
    Open access
  27. Nasima Kanwal, Henri Colaux, Daniel M. Dawson, Yusuke Nishiyama, and Sharon E. Ashbrook
    Sensitivity improvement in 5QMAS NMR experiments using FAM-N pulses,
    Solid State Nucl. Magn. Reson. 100, 1-10 (2019).
    Open Access
  28. Aiyong Wang, Ying Chen, Eric D. Walter, Nancy M. Washton, Donghai Mei, Tamas Varga, Yilin Wang, János Szanyi, Yong Wang, Charles H. F. Peden, and Feng Gao
    Unraveling the mysterious failure of Cu/SAPO-34 selective catalytic reduction catalysts,
    Nat. Commun. 10, article number:1137 (2019).
    Open Access
  29. Bodo Zibrowius and Michael Felderhoff
    On the preparation and NMR spectroscopic characterization of potassium aluminium tetrahydride KAlH4,
    Phys. Chem. Chem. Phys. 21, 12576-12584 (2019).
  30. ❤ Libor Kobera, Jiri Czernek, Sabina Abbrent, Hana Mackova, Lukas Pavlovec, Jan Rohlicek, and Jiri Brus
    The nature of chemical bonding in Lewis adducts as reflected by 27Al NMR quadrupolar coupling constant: Combined solid-state NMR and quantum chemical approach,
    Inorg. Chem. 57, 7428-7437 (2018).
  31. Sharon E. Ashbrook and Paul Hodgkinson
    Perspective: Current advances in solid-state NMR spectroscopy,
    J Chem. Phys. 149, 040901/1-040901/15 (2018).
  32. Jian Zhi Hu, Xin Zhang, Nicholas R. Jaegers, Chuan Wan, Trent R. Graham, Mary Hu, Carolyn I. Pearce, Andrew R. Felmy, Sue B. Clark, and Kevin M. Rosso
    Transitions in Al coordination during Gibbsite crystallization using high-field 27Al and 23Na MAS NMR spectroscopy,
    J. Phys. Chem. C 121, 27555-27562 (2017).
  33. Henri Colaux, Daniel M. Dawson, and Sharon E. Ashbrook
    Investigating FAM-N pulses for signal enhancement in MQMAS NMR of quadrupolar nuclei,
    Solid State Nucl. Magn. Reson. 84, 89-102 (2017).
    Open access
  34. Marcos de Oliveira, Jr., Tássia S. Gonçalves, Cynthia Ferrari, Claudio José Magon, Paulo S. Pizani, Andrea S. S. de Camargo, and Hellmut Eckert
    Structure−property relations in fluorophosphate glasses: An integrated spectroscopic strategy,
    J. Phys. Chem. C 121, 2968-2986 (2017).
  35. Jiri Brus, Sabina Abbrent, Libor Kobera, Martina Urbanova, and Pavel Cuba
    Advances in 27Al MAS NMR studies of geopolymers,
    Annu. Rep. Nucl. Magn. Reson. Spectrosc. 88, 79-147 (2016).
  36. T. Bräuniger, B. Groh, I. L. Moudrakovski, and S. Indris
    Local electronic structure in γ‑LiAlO2 studied by single-crystal 27Al NMR and DFT calculations,
    J. Phys. Chem. A 120, 7839-7846 (2016).
  37. Flaviu R. V. Turcu, Ago Samoson, Maria Maier, Diana L. Trandafir, and Simion Simon
    High fraction of penta-coordinated aluminum and gallium in lanthanum–aluminum–gallium borates,
    J. Am. Ceram. Soc. 99, 2795-2800 (2016).
  38. Marios S. Katsiotis, Michael Fardis, Yasser Al Wahedi, Samuel Stephen, Vasilios Tzitzios, Nikolaos Boukos, Hae Jin Kim, Saeed M. Alhassan, and Georgios Papavassiliou
    Water coordination, proton mobility, and Lewis acidity in HY nanozeolites: A high-temperature 1H and 27Al NMR study,
    J. Phys. Chem. C 119, 3428−3438 (2015).
  39. Jiří Brus, Libor Kobera, Wolfgang Schoefberger, Martina Urbanová, Petr Klein, Petr Sazama, Edyta Tabor, Stepan Sklenak, Anna V. Fishchuk, and Jir Dědeček
    Structure of framework aluminum Lewis sites and perturbed aluminum atoms in zeolites as determined by 27Al{1H} REDOR (3Q) MAS NMR spectroscopy and DFT/molecular mechanics,
    Angew. Chem. Int. Ed. 54, 541-545 (2015).
  40. Xiaochun Zhu, Leilei Wu, Pieter C.M.M. Magusin, Brahim Mezari, and Emiel J.M. Hensen
    On the synthesis of highly acidic nanolayered ZSM-5,
    J. Catal. 327, 10-21 (2015).
  41. Xiong Su, Shutao Xu, Peng Tian, Jinzhe Li, Anmin Zheng, Qiang Wang, Miao Yang, Yingxu Wei, Feng Deng, and Zhongmin Liu
    Investigation of the strong Brønsted acidity in a novel SAPO-type molecular sieve, DNL-6,
    J. Phys. Chem. C 119, 2589-2596 (2015).
  42. K. Keller, E. Brendler, S. Schmerler, C. Röder, G. Heide, J. Kortus, and E. Kroke
    Spectroscopic characterization of rocksalt-type aluminum nitride,
    J. Phys. Chem. C 119, 12581-12588 (2015).
  43. Valerie R. Seymour, Eike C. V. Eschenroeder, Paul A. Wright, and Sharon E. Ashbrook
    An NMR crystallographic approach to monitoring cation substitution in the aluminophosphate STA-2,
    Solid State Nucl. Magn. Reson. 65, 64-74 (2015).
  44. A. Malki, Z. Mekhalif, S. Detriche, G. Fonder, A. Boumaza, and A. Djelloul
    Calcination products of gibbsite studied by X-ray diffraction, XPS and solid-state NMR,
    J. Solid State Chem. 215, 8-15 (2014).
  45. Eric G. Sorte, Samuel B. Emery, E. H. Majzoub, Tim Ellis-Caleo, Zayd L. Ma, Blake A. Hammann, Sophia E. Hayes, Robert C. Bowman, Jr., and Mark S. Conradi
    NMR study of anion dynamics in solid KAlH4,
    J. Phys. Chem. C 118, 5725-5732 (2014).
  46. A. Baasner, B. C. Schmidt, R. Dupree, and S. L. Webb
    Fluorine speciation as a function of composition in peralkaline and peraluminous Na2O–CaO–Al2O3–SiO2 glasses: A multinuclear NMR study,
    Geochim. Cosmochim. Acta 132, 151-169 (2014).
  47. Cornelia Schröder, Jinjun Ren, Ana Candida M. Rodrigues, and Hellmut Eckert
    Glass-to-crystal transition in Li1+xAlxGe2−x(PO4)3: Structural aspects studied by solid state NMR,
    J. Phys. Chem. C 118, 9400-9411 (2014).
  48. Min Bum Park, Aurélie Vicente, Christian Fernandez, and Suk Bong Hong
    Solid-state NMR study of various mono- and divalent cation forms of the natural zeolite natrolite,
    Phys. Chem. Chem. Phys. 15, 7604-7612 (2013).
  49. Chiara Ferrara, Cristina Tealdi, Alfonso Pedone, Maria Cristina Menziani, Aaron J. Rossini, Guido Pintacuda, and Piercarlo Mustarelli
    Local versus average structure in LaSrAl3O7: A NMR and DFT investigation,
    J. Phys. Chem. C 117, 23451-23458 (2013).
  50. G. Ipek Yucelen, Rudra Prosad Choudhury, Johannes Leisen, Sankar Nair, and Haskell W. Beckham
    Defect structures in aluminosilicate single-walled nanotubes: A solid-state nuclear magnetic resonance investigation,
    J. Phys. Chem. C 116, 17149-17157 (2012).
  51. Aaron Palke, Jonathan F. Stebbins, Dan J. Frost, and Catherine A. McCammon
    Incorporation of Fe and Al in MgSiO3 perovskite: An investigation by 27Al and 29Si NMR spectroscopy,
    Am. Mineral. 97, 1955-1964 (2012).
  52. C. Martineau, B. Bouchevreau, F. Taulelle, J. Trebosc, O. Lafon, and J.-P. Amoureux
    High-resolution through-space correlations between spin-1/2 and half-integer quadrupolar nuclei using the MQ-D-R-INEPT NMR experiment,
    Phys. Chem. Chem. Phys. 14, 7112-7119 (2012).
  53. Dennis L. A. G. Grimminck, Ben J. W. Polman, Arno P. M. Kentgens, and W. Leo Meerts
    EASY-GOING deconvolution: Combining accurate simulation and evolutionary algorithms for fast deconvolution of solid-state quadrupolar NMR spectra,
    J. Magn. Reson. 211, 114-120 (2011).
  54. Lu Zhang, Jennifer Bates, Donghan Chen, Heng-Yong Nie, and Yining Huang
    Investigations of formation of molecular sieve SAPO-34,
    J. Phys. Chem. C 115, 22309-22319 (2011).
  55. Charlotte Martineau, Franck Engelke, and Francis Taulelle
    Multiple resonance heteronuclear decoupling under MAS: Dramatic increase of spectral resolution at moderate magnetic field and MAS frequencies,
    J. Magn. Reson. 212, 311-319 (2011).
  56. Ernst R. H. van Eck, Johannis A. Z. Pieterse, and Arno P. M. Kentgens
    Framework and extra-framework aluminium in wet ion exchanged Fe-ZSM5 and the effect of steam during the decomposition of N2O,
    Solid State Nucl. Magn. Reson. 39, 99-105 (2011).
  57. T. Bräuniger, C. Vinod Chandran, U. Wedig, and M. Jansen
    NMR chemical shift and quadrupolar interaction parameters of carbon- coordinated 27Al in aluminium carbide, Al4C3,
    Z. Anorg. Allg. Chem. 637, 530-535 (2011).
  58. Dinu Iuga
    Double-quantum homonuclear correlations of spin I = 5/2 nuclei,
    J. Magn. Reson. 208, 225-234 (2011).
  59. Xianyu Xue
    Determination of J coupling constants between spin-1/2 and quadrupolar nuclei in inorganic solids from spin echo and refocused INEPT experiments: A case study on AlPO4 berlinite,
    Solid State Nucl. Magn. Reson. 38, 62-73 (2010).
  60. Margriet H. W. Verkuijlen, Jinbao Gao, Philipp Adelhelm, P. Jan M. van Bentum, Petra E. de Jongh, and Arno P. M. Kentgens
    Solid-state NMR studies of the local structure of NaAlH4/C nanocomposites at different stages of hydrogen desorption and rehydrogenation,
    J. Phys. Chem. C 114, 4683-4692 (2010).
  61. E. J. M. Hensen , D. G. Poduval, P. C. M. M. Magusin, A. E. Coumans, and J. A. R. van Veen
    Formation of acid sites in amorphous silica-alumina,
    J. Catal. 269, 201-218 (2010).
  62. Edward W. Hagaman, Jian Jiao, Banghao Chen, Zhen Ma, Hongfeng Yin, and Sheng Dai
    Surface alumina species on modified titanium dioxide: A solid-state 27Al MAS and 3QMAS NMR investigation of catalyst supports,
    Solid State Nucl. Magn. Reson. 37, 82-90 (2010).
  63. Nicolas Malicki, Gregor Mali, Anne-Agathe Quoineaud, Patrick Bourges, Laurent J. Simon, Frédéric Thibault-Starzyk, and Christian Fernandez
    Aluminium triplets in dealuminated zeolites detected by 27Al NMR correlation spectroscopy,
    Micropor. Mesopor. Mat. 129, 100-105 (2010).
  64. Shenhui Li, Anmin Zheng, Yongchao Su, Hanjun Fang, Wanling Shen, Zhiwu Yu, Lei Chen, and Feng Deng
    Extra-framework aluminium species in hydrated faujasite zeolite as investigated by two-dimensional solid-state NMR spectroscopy and theoretical calculations,
    Phys. Chem. Chem. Phys. 12, 3895-3903 (2010).
  65. P. Jeglič, S. Vrtnik, M. Bobnar, M. Klanjšek, B. Bauer, P. Gille, Yu. Grin, F. Haarmann, and J. Dolinšek
    M–Al–M groups trapped in cages of Al13M4 (M = Co, Fe, Ni, Ru) complex intermetallic phases as seen via NMR,
    Phys. Rev. B 82, 104201/1-104201/10 (2010).
  66. Mattias Edén
    Two-dimensional MAS NMR correlation protocols involving double-quantum filtering of quadrupolar spin-pairs,
    J. Magn. Reson. 204, 99-110 (2010).
  67. Anastasia Vyalikh, Francis Reny Costa, Udo Wagenknecht, Gert Heinrich, Dominique Massiot, and Ulrich Scheler
    From layered double hydroxides to layered double hydroxide-based nanocomposites--A solid-state NMR study,
    J. Phys. Chem. C 113, 21308-21313 (2009).
  68. Kimberly E. Kelsey, Jonathan F. Stebbins, David M. Singer, Gordon E. Brown Jr., Jed L. Mosenfelder, and Paul D. Asimow
    Cation field strength effects on high pressure aluminosilicate glass structure: Multinuclear NMR and La XAFS results,
    Geochim. Cosmochim. Acta 73, 3914-3933 (2009).
  69. C. M. Morais, V. Montouillout, M. Deschamps, D. Iuga, F. Fayon, F. A. A. Paz, J. Rocha, C. Fernandez, and D. Massiot
    1D to 3D NMR study of microporous alumino-phosphate AlPO4-40,
    Magn. Reson. Chem. 47, 942-947 (2009).
  70. Bruce G. Aitken, Randall E. Youngman, Rashmi R. Deshpande, and Hellmut Eckert
    Structure-property relations in mixed-network glasses: Multinuclear solid state NMR investigations of the system xAl2O3:(30 - x)P2O5:70SiO2,
    J. Phys. Chem. 113, 3322-3331 (2009).
  71. Zhimin Yan, Banghao Chen, and Yining Huang
    A solid-state NMR study of the formation of molecular sieve SAPO-34,
    Solid State Nucl. Magn. Reson. 35, 49-60 (2009).
  72. A. Kuhn, E. Tobschall, and P. Heitjans
    Li ion diffusion in nanocrystalline and nanoglassy LiAlSi2O6 and LiBO2 – Structure-dynamics relations in two glass forming compounds ,
    Z. Phys. Chem. 223, 1359-1377 (2009).
  73. Q. Wang, B. Hu, O. Lafon, J. Trébosc, F. Deng, and J. P. Amoureux
    Double-quantum homonuclear NMR correlation spectroscopy of quadrupolar nuclei subjected to magic-angle spinning and high magnetic field, (BR221; SR221)
    J. Magn. Reson. 200, 251-260 (2009).
  74. A. J. Lussier, P. M. Aguiar, V. K. Michaelis, S. Kroeker, and F. C. Hawthorne
    The occurence of tetrahedrally coordinated Al and B in tourmaline: An 11B and 27Al MAS NMR study,
    Am. Mineral. 94, 785-792 (2009).
  75. Amanpreet Saini, Atul Khanna, Vladimir K. Michaelis, Scott Kroeker, Fernando González, and David Hernández
    Structure-property correlations in lead borate and borosilicate glasses doped with aluminium oxide,
    J. Non-Cryst. Solids 355, 2323-2332 (2009).
  76. William J. Brouwer, Michael C. Davis, and Karl T. Mueller
    Optimized multiple quantum MAS lineshape simulations in solid state NMR,
    Comput. Phys. Commun. 180, 1973-1982 (2009).
  77. Sharon E. Ashbrook
    Recent advances in solid-state NMR spectroscopy of quadrupolar nuclei,
    Phys. Chem. Chem. Phys. 11, 6892-6905 (2009).
  78. Anastasia Vyalikh, Dominique Massiot, and Ulrich Scheler
    Structural characterisation of aluminium layered double hydroxides by 27Al solid-state NMR,
    Solid State Nucl. Magn. Reson. 36, 19-23 (2009).
  79. Shin-Jong Huang, Shang-Bin Liu, and Jerry C .C. Chan
    Heteronuclear dipolar recoupling of half-integer quadrupole nuclei under fast magic angle spinning,
    Solid State Nucl. Magn. Reson. 36, 110-117 (2009).
  80. Mattias Edén
    Homonuclear dipolar recoupling of half-integer spin quadrupolar nuclei: Techniques and applications,
    Solid State Nucl. Magn. Reson. 36, 1-10 (2009).
  81. Takafumi Takahashi, Koji Kanehashi, Yuichi Shimoikeda, Takahiro Nemoto, and Koji Saito
    Practical comparison of sensitivity and resolution between STMAS and MQMAS for 27Al,
    J. Magn. Reson. 198, 228-235 (2009).
  82. Renée Siegel, João Rocha, and Luís Mafra
    Combining STMAS and CRAMPS NMR spectroscopy: High-resolution HETCOR NMR spectra of quadrupolar and 1H nuclei in solids,
    Chem. Phys. Lett. 470, 337-341 (2009).
  83. A. P. M. Kentgens, J. Bart, P. J. M. van Bentum, A. Brinkmann, E. R. H. van Eck, J. G. E. Gardeniers, J. W. G. Janssen, P. Knijn, S. Vasa, and M. H. W. Verkuijlen
    High-resolution liquid- and solid-state nuclear magnetic resonance of nanoliter sample volumes using microcoil detectors,
    J Chem. Phys. 128, 052202/1-052202/17 (2008).
  84. Andreas Brinkmann, Arno P. M. Kentgens, Tiit Anupõld, and Ago Samoson
    Symmetry-based recoupling in double-rotation NMR spectroscopy,
    J. Chem. Phys. 129, 174507/1-174507/11 (2008).
  85. R. Hajjar, Y. Millot, P. P. Man, M. Che, and S. Dzwigaj
    Two kinds of framework Al sites studied in BEA zeolite by X-ray diffraction, Fourier transform infrared spectroscopy, NMR techniques, and V probe,
    J. Phys. Chem. C 112, 20167-20175 (2008).
  86. H. M. Kao, P. C. Chang, Y. W. Liao, L. P. Lee, and C. H. Chien
    Solid-state NMR characterization of the acid sites in cubic mesoporous Al-MCM-48 materials using trimethylphosphine oxide as a 31P NMR probe,
    Microporous Mesoporous Mater. 114, 352-364 (2008).
  87. G. L. Kennedy, J. W. Wiench, and M. Pruski
    Determination of 27Al-29Si connectivities in zeolites with 2D 27Al -> 29Si RAPT-CPMG-HETCOR NMR,
    Solid State Nucl. Magn. Reson. 33, 76-81 (2008).
  88. B. Xu, S. Bordiga, R. Prins, and J. A. van-Bokhoven
    Effect of framework Si/Al ratio and extra-framework aluminum on the catalytic activity of Y zeolite,
    Appl. Catal. A 333, 245-253 (2008).
  89. E. S. Mananga, C. D. Hsu, S. Ishmael, T. Islam, and G. S. Boutis
    Probing the validity of average Hamiltonian theory for spin I = 1, 3/2 and 5/2 nuclei by analyzing a simple two-pulse sequence,
    J. Magn. Reson. 193, 10-22 (2008).
  90. J. H. Kwak, J. Z. Hu, A. Lukaski, D. H. Kim, J. Szanyi, and C. H. F. Peden
    Role of pentacoordinated Al3+ ions in the high temperature phase transformation of gamma-Al2O3,
    J. Phys. Chem. C 112, 9486-9492 (2008).
  91. M. Goswami and P. K. Madhu
    Sensitivity enhancement of the central-transition signal of half-integer spin quadrupolar nuclei in solid-state NMR: Features of multiple fast amplitude-modulated pulse transfer,
    J. Magn. Reson. 192, 230-234 (2008).
  92. J. B. D. de-Lacaillerie, C. Fretigny, and D. Massiot
    MAS NMR spectra of quadrupolar nuclei in disordered solids: The Czjzek model,
    J. Magn. Reson. 192, 244-251 (2008).
  93. G. Mali, V.Kaucic, and F. Taulelle
    Measuring distances between half-integer quadrupolar nuclei and detecting relative orientations of quadrupolar and dipolar tensors by double-quantum homonuclear dipolar recoupling nuclear magnetic resonance experiments,
    J. Chem. Phys. 128, 204503/1-204503/11 (2008).
  94. B. Hu, J. P. Amoureux, J. Trebosc, and S. Hafner
    Through-space MP-CPMAS experiments between spin-1/2 and half-integer quadrupolar nuclei in solid-state NMR,
    J. Magn. Reson. 192, 8-16 (2008).
  95. X. Y. Xue and M. Kanzaki
    Structure of hydrous aluminosilicate glasses along the diopside-anorthite join: A comprehensive one- and two-dimensional 1H and 27Al NMR study,
    Geochim. Cosmochim. Acta 72, 2331-2348 (2008).
  96. R. Hajjar, Y. Millot, and P. P. Man
    NMR experimental procedure for obtaining 3Q and 5QMAS spectra from the same multiplex SPAM acquisition,
    C. R. Chim. 11, 380-386 (2008).
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    Characterization of mesoporous alumina prepared by surface alumination of SBA-15,
    Microporous Mesoporous Mater. 110, 232-241 (2008).
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    Structural environments for boron and aluminum in alumina-boria catalysts and their precursors from 11B and 27Al single- and double-resonance MAS NMR experiments,
    J. Phys. Chem. C 112, 7210-7222 (2008).
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    Structural and reactive relevance of V + Nb coverage on alumina of V-Nb-O/Al2O3 catalytic systems,
    J. Catal. 255, 94-103 (2008).
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    Olefin metathesis over heterogeneous catalysts: Interfacial interaction between Mo species and a Hβ - Al2O3 composite support,
    J. Phys. Chem. C 112, 5955-5960 (2008).
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    Characterization and acidic properties of aluminum-exchanged zeolites X and Y,
    J. Phys. Chem. C 112, 3811-3818 (2008).
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    Spin-counting NMR experiments for the spectral editing of structural motifs in solids,
    Phys. Chem. Chem. Phys. 10, 1298-1303 (2008).
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    A practical comparison of MQMAS techniques,
    Solid State Nucl. Magn. Reson. 32, 99-108 (2008).
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    Measurement of through-space connectivities between spin-1/2 and quadrupolar nuclei in solid-state NMR: the TEDOR-MQMAS method,
    Magn. Reson. Chem. 45, S187-S191 (2008).
  105. A. Quintas, T. Charpentier, O. Majérus, D. Caurant, J.-L. Dussossoy, and P. Vermaut
    NMR study of a rare-earth aluminoborosilicate glass with varying CaO-to-Na2O ratio,
    Appl. Magn. Reson. 32, 613-634 (2007).
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    Al speciation in tropical podzols of the upper Amazon Basin: A solid-state 27Al MAS and MQMAS NMR study,
    Geochim. Cosmochim. Acta 71, 3211-3222 (2007).
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    High-pressure δ-Al(OH)3 and δ-AlOOH phases and isostructural hydroxides/oxyhydroxides: New structural insights from high-resolution 1H and 27Al NMR,
    J. Phys. Chem. B 111, 13156-13166 (2007).
  108. X. J. Li, W. P. Zhang, S. L. Liu, L. Y. Xu, X. W. Han, and X. H. Bao
    The role of alumina in the supported Mo/HBeta-Al2O3 catalyst for olefin metathesis: A high-resolution solid-state NMR and electron microscopy study,
    J. Catal. 250, 55-66 (2007).
  109. N. Pellerin, C. Dodane-Thiriet, V. Montouillout, M. Beauvy, and D. Massiot
    Cation sublattice disorder induced by swift heavy ions in MgAl2O4 and ZnAl2O4 spinels: 27Al solid-state NMR study,
    J. Phys. Chem. B 111, 12707-12714 (2007).
  110. M. F. Williams, B. Fonfe, C. Sievers, A. Abraham, J. A. van-Bokhoven, A. Jentys, J. A. R. van-Veen, and J. A. Lercher
    Hydrogenation of tetralin on silica-alumina-supported Pt catalysts I. Physicochemical characterization of the catalytic materials,
    J. Catal. 251, 485-496 (2007).
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    Aluminum siting in silicon-rich zeolite frameworks: A combined high-resolution 27Al NMR spectroscopy and quantum mechanics/molecular mechanics study of ZSM-5,
    Angew. Chem. Int. Ed. 46, 7286-7289 (2007).
  112. L. van-Wullen, G. Tricot, and S. Wegner
    An advanced NMR protocol for the structural characterization of aluminophosphate glasses,
  113. J. H. Kwak, J. Z. Hu, D. H. Kim, J. Szanyi, and C. H. F. Peden
    Penta-coordinated Al3+ ions as preferential nucleation sites for BaO on γ-Al2O3: An ultra-high-magnetic field 27Al MAS NMR study,
    J. Catal. 251, 189-194 (2007).
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    27Al NMR study of the structure of lanthanum- and yttrium-based aluminosilicate glasses and melts,
    J. Phys. Chem. B 111, 9747-9757 (2007).
  115. N. G. Karpukhina, U. Werner-Zwanziger, J. W. Zwanziger, and A. A. Kiprianov
    Preferential binding of fluorine to aluminum in high peralkaline aluminosilicate glasses,
    J. Phys. Chem. B 111, 10413-10420 (2007).
  116. A. Montesinos-Castellanos, E. Lima, J. A. de-los-Reyes, and L. Lara
    Fractal dimension of MoP-Al2O3 catalysts and their activity in hydrodesulfurization of dibenzothiophene,
    J. Phys. Chem. B 111, 13898-13904 (2007).
  117. D. Mohr, A. S. S. de-Camargo, C. C. de-Araujo, and H. Eckert
    Local environment of scandium in aluminophosphate laser glasses: structural studies by solid state NMR spectroscopy,
    J. Mater. Chem. 17, 3733-3738 (2007).
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    Structural role of fluoride in aluminophosphate sol-gel glasses: High-resolution double-resonance NMR studies,
    J. Phys. Chem. B 111, 10402-10412 (2007).
  119. K. A. Denkenberger, R. A. Bowers, A. D. Jones, and K. T. Mueller
    NMR studies of the thermal degradation of a perfluoropolyether on the surfaces of gamma-alumina and Kaolinite,
    Langmuir 23, 8855-8860 (2007).
  120. T. J. Ball and S. Wimperis
    Use of SPAM and FAM pulses in high-resolution MAS NMR spectroscopy of quadrupolar nuclei,
    J. Magn. Reson. 187, 343-351 (2007).
  121. V. Šepelák, S. Indris, I. Bergmann, A. Feldhoff, K. D. Becker, and P. Heitjans
    Nonequilibrium cation distribution in nanocrystalline MgAl2O4 spinel studied by 27Al magic-angle spinning NMR,
    Solid State Ionics 177, 2487-2490 (2006).
  122. M. Afeworki, G. Cao, D. L. Dorset, K. G. Strohmaier, and G. J. Kennedy
    Multinuclear and multidimensional solid-state NMR characterization of EMM-8,
    Microporous Mesoporous Mater. 103, 216-224 (2007).
  123. J. Trebosc, B. Hu, J. P. Amoureux, and Z. Gan
    Through-space R3-HETCOR experiments between spin-1/2 and half-integer quadrupolar nuclei in solid-state NMR,
    J. Magn. Reson. 186, 220-227 (2007).
  124. F. Angeli, M. Gaillard, P. Jollivet, and T. Charpentier
    Contribution of 43Ca MAS NMR for probing the structural configuration of calcium in glass,
    Chem. Phys. Lett. 440, 324-328 (2007).
  125. L. van-Wullen, S. Wegner, and G. Tricot
    Structural changes above the glass transition and crystallization in aluminophosphate glasses: An in situ high-temperature MAS NMR study,
    J. Phys. Chem. B 111, 7529-7534 (2007).
  126. J. Xu, L. Chen, D. L. Zeng, J. Yang, M. J. Zhang, C. H. Ye, and F. Deng
    Crystallization of AlPO4-5 aluminophosphate molecular sieve prepared in fluoride medium: A multinuclear solid-state NMR study,
    J. Phys. Chem. B 111, 7105-7113 (2007).
  127. L. Zhang, C. C. de-Araujo, and H. Eckert
    Aluminum lactate - An attractive precursor for sol-gel synthesis of alumina-based glasses,
    J. Non-Cryst. Solids 353, 1255-1260 (2007).
  128. L. Delevoye, J. Trebosc, Z. Gan, L. Montagne, and J. P. Amoureux
    Resolution enhancement using a new multiple-pulse decoupling sequence for quadrupolar nuclei,
    J. Magn. Reson. 186, 94-99 (2007).
  129. V. Rodriguez-Gonzalez, R. Gomez, M. Moscosa-Santillan, and J. Amouroux
    Sol-gel preparation of In2O3-Al2O3 supports with controlled textural and structural properties,
    React. Kinet. Catal. Lett. 90, 331-338 (2007).
  130. J. Trebosc, J.-P. Amoureux, and Z. H. Gan
    Comparison of high-resolution solid-state NMR MQMAS and STMAS methods for half-integer quadrupolar nuclei,
    Solid State Nucl. Magn. Reson. 31, 1-9 (2007).
  131. X. Y. Xue and M. Kanzaki
    Al coordination and water speciation in hydrous aluminosilicate glasses: Direct evidence from high-resolution heteronuclear 1H-27Al correlation NMR,
    Solid State Nucl. Magn. Reson. 31, 10-27 (2007).
  132. J. F. Stebbins
    Aluminum substitution in rutile titanium dioxide: New constraints from high-resolution 27Al NMR,
    Chem. Mater. 19, 1862-1869 (2007).
  133. M. Igarashi, T. Kodaira, T. Shimizu, A. Goto, K. Hashi, T. Nakano, Y. Nozue
    Anomalous property of the spin-spin relaxation of 27Al NMR in dehydrated zeolite A,
    Chem. Phys. Lett. 436, 80-83 (2007).
  134. H. J. Kim, H. C. Lee, and J. S. Lee
    27Al triple-quantum magic-angle spinning nuclear magnetic resonance characterization of nanostructured alumina materials,
    J. Phys. Chem. C 111, 1579-1583 (2007).
  135. Y. Cai, R. Kumar, W. Huang, B. G. Trewyn, J. W. Wiench, M. Pruski, and V. S. Y. Lin
    Mesoporous aluminum silicate catalyst with single-type active sites: Characterization by solid-state NMR and studies of reactivity for Claisen rearrangement reactions,
    J. Phys. Chem. C 111, 1480-1486 (2007).
  136. H. M. Kao and Y. C. Liao
    Direct solid-state NMR observation of tetrahedral aluminum fluorides in zeolite HY fluorinated by ammonium fluoride,
    J. Phys. Chem. C 111, 4495-4498 (2007).
  137. T. Vosegaard and D. Massiot
    High-resolution two-dimensional NMR spectra of half-integer-spin quadrupolar nuclei from one-dimensional projections,
    Chem. Phys. Lett. 437, 120-125 (2007).
  138. E. V. Charnaya, C. Tien, N. V. Chejina, M. K. Lee, and S. Y. Sun
    Effect of alkali-earth ions on the local structure LaAlO3-La0.67A0.33MnO3 (A = Ca,Sr,Ba) diluted solid solutions: 27Al NMR studies,
    Phys. Solid State 49, 449-453 (2007).
  139. D. R. Neuville, L. Cormier, V. Montouillout, and D. Massiot
    Local Al site distribution in aluminosilicate glasses by 27Al MQMAS NMR,
    J. Non-Cryst. Solids 353, 180-184 (2007).
  140. J. P. Amoureux, J. Trebosc, J. Wiench, and M. Pruski
    HMQC and refocused-INEPT experiments involving half-integer quadrupolar nuclei in solids,
    J. Magn. Reson. 184, 1-14 (2007).
  141. D. Vuono, L. Pasqua, F. Testa, R. Aiello, A. Fonseca, T. I. Koranyi, and J. B. Nagy
    Influence of NaOH and KOH on the synthesis of MCM-22 and MCM-49 zeolites,
    Microporous Mesoporous Mater. 97, 78-87 (2007).
  142. R. Siegel, T. T. Nakashima, and R. E. Wasylishen
    Sensitivity enhancement of NMR spectra of half-integer spin quadrupolar nuclei in solids using hyperbolic secant pulses,
    J. Magn. Reson. 184, 85-100 (2007).
  143. P. Florian, E. M. Anghel, and C. Bessada
    Structural description of the Na2B4O7-Na3AlF6-TiO2 system. 2. A multinuclear NMR approach of melts and solids,
    J. Phys. Chem. B 111, 968-978 (2007).
  144. M. Deschamps and D. Massiot
    Three-dimensional through-bond homonuclear-heteronuclear correlation experiments for quadrupolar nuclei in solid-state NMR applied to 27Al-O-31P-O-27Al networks,
    J. Magn. Reson. 184, 15-19 (2007).
  145. G. Cao, M. Afeworki, G. J. Kennedy, K. G. Strohmaier, and D. L. Dorset
    Structure of an aluminophosphate EMM-8: a multi-technique approach,
    Acta Cryst. B 63, 56-62 (2007).
  146. J. G. Longstaffe, B. H. Chen, and Y. N. Huang
    Characterization of the amorphous phases formed during the synthesis of microporous material AlPO4-5,
    Microporous Mesoporous Mater. 98, 21-28 (2007).
  147. R. Roldan, M. Sanchez-Sanchez, G. Sankar, F. J. Romero-Salguero, C. Jimenez-Sanchidrian
    Influence of pH and Si content on Si incorporation in SAPO-5 and their catalytic activity for isomerisation of n-heptane over Pt loaded catalysts,
    Microporous Mesoporous Mater. 99, 288-298 (2007).
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    Structural study of VOx doped aluminium fluoride and aluminium oxide catalysts,
    Solid State Chem. 180, 749-758 (2007).

Related bibliography

  1. P. J. Carl, D. E. W. Vaughan, and D. Goldfarb
    High field 27Al ENDOR reveals the coordination mode of Cu2+ in low Si/Al zeolites,
    J. Am. Chem. Soc. 128, 7160-7161 (2006).
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