Satellite Transition Magic Angle Spinning references
Below are provided some NMR references about ST-MAS
applied to half-integer quadrupole spins. These references contain
(1) the pulse-sequence diagram,
(2) the coherence-transfer pathways,
(3) the phase-cycling,
(4) the receiver-phase relationship.
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Takafumi Takahashi, Shunsuke Kashiwakura, Koji Kanehashi, and Tetsuya Nagasaka
First high-resolution 11B nuclear magnetic resonance (NMR) spectra of coal fly ash by satellite-transition magic angle spinning (STMAS) NMR, (1)(2)
Energy Fuels 23, 1778-1780 (2009).
Abstract -
Takafumi Takahashi, Koji Kanehashi, Yuichi Shimoikeda, Takahiro Nemoto, and Koji Saito
Practical comparison of sensitivity and resolution between STMAS and MQMAS for 27Al, (1)(2)(3)
J. Magn. Reson. 198, 228-235 (2009).
Abstract -
J. Trebosc, J.-P. Amoureux, and Z. H. Gan
Comparison of high-resolution solid-state NMR MQMAS and STMAS methods for half-integer quadrupolar nuclei, (1)
Solid State Nucl. Magn. Reson. 31, 1-9 (2007). -
J.-P. Amoureux and J. Trébosc
Homogeneous broadenings in 2D solid-state NMR of half-integer quadrupolar nuclei, (1)(2)
J. Magn. Reson. 179, 311-316 (2006). -
O. B. Lapina, D. F. Khabibulin, K. V. Romanenko, Z. H. Gan, M. G. Zuev,
V. N. Krasil'nikov, and V. E. Fedorov
93Nb NMR chemical shift scale for niobia systems,
Solid State Nucl. Magn. Reson. 28, 204-224 (2005). -
J.-P. Amoureux, A. Flambard, L. Delevoye, and L. Montagne
A very sensitive high-resolution NMR method for quadrupolar nuclei: SPAM-DQF-STMAS, (1)(2)
Chem. Commun.3472-3474 (2005). -
J.-P. Amoureux, L. Delevoye, G. Fink, F. Taulelle, A. Flambard, and L. Montagne
Implementing SPAM into STMAS: a net sensitivity improvement in high-resolution NMR of quadrupolar nuclei, (1)(2)(3)
J. Magn. Reson. 175, 285-299 (2005). -
Sharon E. Ashbrook and Stephen Wimperis,
High-resolution NMR of quadrupolar nuclei in solids: the satellite-transition magic angle spinning (STMAS) experiment, (1)(2)(3)
Progr. Nucl. Magn. Reson. Spectrosc. 45, 53-108 (2004). -
N. G. Dowell, S. E. Ashbrook, and S. Wimperis
Satellite-transition MAS NMR of low-gamma nuclei at natural abundance: sensitivity, practical implementation, and application to 39K (I = 3/2) and 25Mg (I = 5/2), (1)(2)
J. Phys. Chem. B 108, 13292-13299 (2004). -
Z. Gan, P. Srinivasan, J. R. Quine, S. Steuernagel, and B. Knott
Third-order effect in solid-state NMR of quadrupolar nuclei,
Chem. Phys. Lett. 367, 163-169 (2003). -
J.-P. Amoureux, C. Morais, J. Trebosc, J. Rocha, and C. Fernandez
I-STMAS, a new high-resolution solid-state NMR method for half-integer, (1)(2)(3)
Solid State Nucl. Magn. Reson. 23, 213-223 (2003). -
S. Wi, S. E. Ashbrook, S. Wimperis, L. Frydman
Second-order quadrupole-shielding effects in magic-angle spinning solid-state nuclear magnetic resonance,
J. Chem. Phys. 118, 3131-3140 (2003). -
H. T. Kwak and Z. H. Gan
Double-quantum filtered STMAS, (1)(2)(3)
J. Magn. Reson. 164, 369-372 (2003). -
S. E. Ashbrook and S. Wimperis
SCAM-STMAS: satellite-transition MAS NMR of quadrupolar nuclei with self-compensation for magic-angle misset, (1)(2)(3)
J. Magn. Reson. 162, 402-416 (2003). -
J.-P. Amoureux, C. Huguenard, F. Engelke, and F. Taulelle
Unified representation of MQMAS and STMAS NMR of half-integer quadrupolar nuclei,
Chem. Phys. Lett. 356, 497-504 (2002). -
S. E. Ashbrook and S. Wimperis
Satellite-transition MAS NMR of spin I = 3/2, 5/2, 7/2, and 9/2 nuclei: sensitivity, resolution, and practical implementation, (1)(2)(3)
J. Magn. Reson. 156, 269-281 (2002). -
C. Huguenard, F. Taulelle, B. Knott, and Z. Gan
Optimizing STMAS, (1)(2)(3)
J. Magn. Reson. 156, 131-137 (2002). -
S. E. Ashbrook and S. Wimperis
High-resolution NMR spectroscopy of quadrupolar nuclei in solids: satellite-transition MAS with self-compensation for magic-angle misset, (1)(2)(3)
J. Am. Chem. Soc. 124, 11602-11603 (2002). -
Z. Gan, P. Gor'kov, T. A. Cross, A. Samoson, and D. Massiot
Seeking higher resolution and sensitivity for NMR of quadrupolar nuclei at ultrahigh magnetic fields,
J. Am. Chem. Soc. 124, 5634-5635 (2002). -
K. J. Pike, S. E. Ashbrook, and S. Wimperis
Two-dimensional satellite-transition MAS NMR of quadrupolar nuclei: shifted echoes, high-spin nuclei and resolution, (1)(2)(3)
Chem. Phys. Lett. 345, 400-408 (2001). -
Z. Gan
Satellite transition magic-angle spinning nuclear magnetic resonance of half-integer quadrupolar nuclei, (1)(2)(3)
J. Chem. Phys. 114, 10845-10853 (2001). -
Z. Gan
Isotopic NMR spectra of half-integer quadrupolar nuclei using satellite transitions and magic-angle spinning, (3)
J. Am. Chem. Soc. 122, 3242-3243 (2000).