1Q-CP MQ-MAS references

Below are provided some NMR references for single-quantum Cross- Polarization followed by MQ-MAS sequence applied to half-integer quadrupole spins. These references contain
(1) the pulse-sequence diagram,
(2) the coherence-transfer pathways,
(3) the phase-cycling.

1. J.-P. Amoureux and M. Pruski,
   Advances in MQMAS NMR, (1)(2)
   in Encyclopedia of Nuclear Magnetic Resonance, edited by D. M. Grant and R. K. Harris,
   (J. Wiley, Chichester, Vol. 9, 226-251, 2002).
2. S. E. Ashbrook and S. Wimperis
   Novel two-dimensional NMR methods that combine single-quantum cross-polarization and MQ-MAS of quadrupolar nuclei, (1)(2)
   Chem. Phys. Lett. 2001, 500-508 (2001).
3. K. H. Lim and C. P. Grey
   ¹⁹F/²³Na multiple quantum cross polarization NMR in solids, (1)(3)
   J. Chem. Phys. 112, 7490-7504 (2000).
4. S. E. Ashbrook and S. Wimperis
   Multiple-quantum cross-polarization and two-dimensional MQMAS NMR of quadrupolar nuclei, (1)(2)
   J. Magn. Reson. 147, 238-249 (2000).
5. M. Pruski, C. Fernandez, D. P. Lang, and J.-P. Amoureux
   Measurement of interatomic connectivities in molecular sieves using MQMAS-based methods, (1)(2)
   Catal. Today 49, 401-409 (1999).
6. F. Taulelle, M. Pruski, J.-P. Amoureux, D. Lang, A. Bailly, C. Huguenard, M. Haouas, C. Gérardin, T. Loiseau, and G. Ferey
   Isomerization of the prenucleation building unit during crystallization of AlPO₄-CJ2: An MQMAS, CP-MQMAS, and HETCOR NMR study, (1)(2)
   J. Am. Chem. Soc. 121, 12148-12153 (1999).
7. C. Fernandez, L. Delevoye, J.-P. Amoureux, D. P. Lang, and M. Pruski
   ²⁷Al{¹H} cross polarization triple-quantum MAS NMR, (1)(3)
   J. Am. Chem. Soc. 119, 6858-6862 (1997).
8. M. Pruski, D. P. Lang, C. Fernandez, and J.-P. Amoureux
   MQ MAS NMR with cross-polarization: Spectral editing of high-resolution spectra of quadrupolar nuclei, (1)(2)
   Solid State Nucl. Magn. Reson. 7, 327-331 (1997).

Related bibliography

1. S. E. Ashbrook and S. Wimperis
   Single- and multiple-quantum cross-polarization in NMR of quadrupolar nuclei in static samples, (1)(2)
   Mol. Phys. 98, 1-26 (2000).
2. A. J. Vega
   CP/MAS of quadrupolar S = 3/2 nuclei,
   Solid State Nucl. Magn. Reson. 1, 17-32 (1992).