References for two-pulse nutation NMR

Two-pulse nutation experiments with a short interpulse delay tau1 are more versatile than one-pulse nutation experiment: A short tau1 avoids the formation of echoes. We can perform two experiments with different acquisition parameters on the same sample.

References containing data and graphs that can be simulated with the two-pulse applets, in order to determine the quadrupole coupling from a featureless NMR lineshape:

1. S. Z. Ageev, P. P. Man, J. Fraissard, and B. C. Sanctuary
   Determination of quadrupolar spin coupling for spin 7/2 using two pulse sequences (PDF article, 181 Kb),
   Mol. Phys. 91, 75-80 (1997).
2. M. A. Hepp, P. P. Man, A. Trokiner, and J. Fraissard
   Determination of the quadrupole coupling from featureless line shapes,
   Magn. Reson. Chem. 32, 24-28 (1994).
3. P. P. Man
   Determination of spin-5/2 quadrupolar coupling with two-pulse sequences,
   Solid State Nucl. Magn. Reson. 2, 165-180 (1993).
4. M. A. Hepp, P. P. Man, A. Trokiner, H. Zanni, and J. Fraissard
   Determination of the electric field gradient in RbCaF₃ near the phase transition (PDF article, 397 Kb),
   Solid State Commun. 84, 869-873 (1992).
5. P. P. Man
   Determination of the quadrupolar coupling constant in powdered samples with a two in-phase rf pulse sequence in solid-state NMR (PDF article, 394 Kb),
   Chem. Phys. Lett. 168, 227-232 (1990).
6. P. P. Man
   Measurement of quadrupolar coupling with a two-pulse sequence in solid-state NMR (PDF article, 425 Kb),
   Mol. Phys. 69, 337-346 (1990).

Related bibliography

1. J. Haase and H. Pfeifer
   A new two-pulse free induction decay method to measure solid-state NMR spectra of quadrupolar nuclei with half-integer spin,
   J. Magn. Reson. 86, 217-226 (1990).
2. J. Haase, D. Freude, H. Pfeifer, E. Lippmaa, and P. Sarv
   Two-pulse free induction decay quadrupole NMR,
   Chem. Phys. Lett. 152, 254-257 (1988).