References for spin lock nutation NMR
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The signal is observed at the end of two consecutive pulses with quadrature phases.
References containing data and graphs that can be simulated with the spin-locking applets, in order to determine the quadrupole coupling from a featureless NMR lineshape, are provided:
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S. Z. Ageev, P. P. Man, and B. C. Sanctuary
Detection of double and four quantum coherences for spin 7/2 excited by spin lock pulse sequences (PDF article, 160 Kb),
J. Magn. Reson. 128, 12-20 (1997). -
P. P. Man
Detection of double-quantum coherences in a spin-5/2 system excited by spin-lock sequences (PDF article, 428 Kb),
J. Magn. Reson. A 113, 40-46 (1995). -
P. P. Man
Double-quantum coherence detection in a spin-3/2 system excited by two consecutive pulses (PDF article, 491 Kb),
Mol. Phys. 76, 1119-1129 (1992).
SIMPSON scripts and Mathematica-5 notebooks
Use Wolfram CDF Player to read Mathematica notebook in modern web browser.
- Effet of offset on spinlock 90°(X)90°(Y) pulse for positive gyromagnetic ratio nucleus:
*magnetization x component,
*magnetization y component,
*magnetization z component,
*corresponding Mathematica 5 notebook. - Composite rotation matrices in Mathematica-5 notebook:
*passive rotation about rotated axes,
*active rotation about rotated axes.