Reference for split-t1 MQ-MAS




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Split-t1 MQ-MAS references

Below are provided some NMR references about MQ-MAS with split-t1 sequence applied to half-integer quadrupole spins. These references contain
(1) the pulse-sequence diagram,
(2) the coherence-transfer pathways,
(3) the phase-cycling,
(4) the receiver-phase relationship.

  • Renée Siegel, T. T. Nakashima, and R. E. Wasylishen
    Sensitivity enhancement of MQMAS NMR spectra of spin 3/2 nuclei using hyperbolic secant pulses, (1)(2)
    Chem. Phys. Lett. 403, 353-358 (2005).
     
  • J. Gu and W. P. Power
    Improved quantitation in 3QMAS of spin 5/2 nuclei by RF power modulation of FAM-II, (1)(2)(3)
    Solid State NMR 27, 192-199 (2005).
     
  • N. G. Dowell, S. E. Ashbrook, and S. Wimperis
    Satellite-transition MAS NMR of low-gamma nuclei at natural abundance: sensitivity, practical implementation, and application to 39K (I = 3/2) and 25Mg (I = 5/2), (1)(2)
    J. Phys. Chem. B 108, 13292-13299 (2004).
     
  • A. Goldbourt, E. Vinogradov, G. Goobes, and S. Vega
    High resolution heteronuclear correlation NMR spectroscopy between quadrupolar nuclei and protons in the solid state, (3)
    J. Magn. Reson. 169, 342-350 (2004).
     
  • T. Bräuniger, K. J. Pike, R. K. Harris, and P. K. Madhu
    Efficient 5QMAS NMR of spin-5/2 nuclei: use of fast amplitude-modulated radio-frequency pulses and cogwheel phase cycling, (1)(2)(3)
    J. Magn. Reson. 163, 64-72 (2003).
     
  • A. Jerschow and R. Kumar
    Calculation of coherence pathway selection and cogwheel cycles, (1)(2)
    J. Magn. Reson. 160, 59-64 (2003).
     
  • A. Goldbourt, M. V. Landau, and S. Vega
    Characterization of aluminum species in alumina multilayer grafted MCM-41 using 27Al FAM(II)-MQMAS NMR, (1)(2)(3)
    J. Phys. Chem. B 107, 724-731 (2003).
     
  • M. H. Levitt, P. K. Madhu, and C. E. Hughes
    Cogwheel phase cycling, (1)(2)(3)
    J. Magn. Reson. 155, 300-306 (2002).
     
  • A. Goldbourt and S. Vega
    Signal enhancement in 5QMAS spectra of spin-5/2 quadrupolar nuclei, (1)(2)(3)
    J. Magn. Reson. 154, 280-286 (2002).
     
  • J.-P. Amoureux and M. Pruski,
    Advances in MQMAS NMR, (1)(2)
    in Encyclopedia of Nuclear Magnetic Resonance, edited by D. M. Grant and R. K. Harris,
    (J. Wiley, Chichester, Vol. 9, 226-251, 2002).
     
  • A. Goldbourt and P. K. Madhu
    Multiple-Quantum Magic Angle Spinning: High-resolution solid state NMR spectroscopy of half-integer quadrupolar nuclei, (1)(2)(3)(4)
    Monatsh. Chem. 133, 1497-1534 (2002).
     
  • A. Jerschow, J. W. Logan, and A. Pines
    High-resolution NMR of quadrupolar nuclei using mixed multiple-quantum coherences, (1)(2)(3)
    J. Magn. Reson. 149, 268-270 (2001).
     
  • S. E. Ashbrook and S. Wimperis
    Novel two-dimensional NMR methods that combine single-quantum cross-polarization and MQ-MAS of quadrupolar nuclei, (1)(2)
    Chem. Phys. Lett. 340, 500-508 (2001).
     
  • T. Vosegaard, D. Massiot, and P. J. Grandinetti
    Sensitivity enhancements in MQ-MAS NMR of spin-5/2 nuclei using modulated RF mixing pulses, (1)(2)(3)
    Chem. Phys. Lett. 326, 454-460 (2000).
     
  • K. J. Pike, R. P. Malde, S. E. Ashbrook, J. McManus, and S. Wimperis
    Multiple-quantum MAS NMR of quadrupolar nuclei. Do five-, seven- and nine-quantum experiments yield higher resolution than the three-quantum experiment?, (1)(2)
    Solid State NMR 16, 203-215 (2000).
     
  • S. E. Ashbrook and S. Wimperis
    Multiple-quantum cross-polarization and two-dimensional MQMAS NMR of quadrupolar nuclei, (1)(2)
    J. Magn. Reson. 147, 238-249 (2000).
     
  • M. Pruski, J. W. Wiench, and J.-P. Amoureux
    On the conversion of triple- to single-quantum coherences in MQMAS NMR, (1)(2)
    J. Magn. Reson. 147, 286-295 (2000).
     
  • S. P. Brown, S. E. Ashbrook, and S. Wimperis
    27Al MQ-MAS NMR study of the thermal transformation between the microporous aluminum methylphosphonates AlMePO-beta and AlMePO-alpha, (1)(2)(3)
    J. Phys. Chem. B 103, 812-817 (1999).
     
  • T. Mildner, M. E. Smith, and R. Dupree
    2D five quantum MAS NMR using rotationally induced coherence transfer, (3)
    Chem. Phys. Lett. 306, 297-302 (1999).
     
  • T. Mildner, M. E. Smith, and R. Dupree
    Rotationally induced triple quantum coherence excitation in MAS NMR spectroscopy of I = 5/2 spins, (1)(3)
    Chem. Phys. Lett. 301, 389-394 (1999).
     
  • S. E. Ashbrook, S. P. Brown, and S. Wimperis
    Multiple-quantum cross-polarization in MAS NMR of quadrupolar nuclei, (1)(2)
    Chem. Phys. Lett. 288, 509-517 (1998).
     
  • S. P. Brown and S. Wimperis
    Two-dimensional MQ-MAS NMR of quadrupolar nuclei: a comparison of methods, (1)(2)(3)
    J. Magn. Reson. 128, 42-61 (1997).
     

Related bibliography

  • Z. H. Gan and H. T. Kwak
    Enhancing MQMAS sensitivity using signals from multiple coherence transfer pathways,
    J. Magn. Reson. 168, 346-351 (2004).
     
 

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[Contact me] - Last updated December 15, 2012
Solid-state NMR bibliography for
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Beryllium-9
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Calcium-43
Cesium-133
Chlorine-35/37
Chromium-53
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Deuterium-2
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Germanium-73
Gold-197
Hafnium-177/179
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Iodine-127
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Krypton-83
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Lithium-7
Magnesium-25
Manganese-55
Mercury-201
Molybdenum-95/97
Neon-21
Nickel-61
Niobium-93
Nitrogen-14
Osmium-189
Oxygen-17
Palladium-105
Potassium-39/41
Rhenium-185/187
Rubidium-85/87
Ruthenium-99/101
Scandium-45
Sodium-23
Strontium-87
Sulfur-33
Tantalum-181
Titanium-47/49
Vanadium-51
Xenon-131
Zinc-67
Zirconium-91



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