Reference for SPAM MQ-MAS




Home and Applets > Pulse Sequence > SPAM MQ-MAS Reference

SPAM MQ-MAS references

Below are provided some NMR references about MQ-MAS with SPAM applied to half-integer quadrupole spins. These references contain
(1) the pulse-sequence diagram,
(2) the coherence-transfer pathways,
(3) the phase-cycling,
(4) the receiver-phase relationship.

  • Zhehong Gan, Peter L. Gor’kov, William W. Brey, Paul J. Sideris, and Clare P. Grey
    Enhancing MQMAS of low-γ nuclei by using a high B1 field balanced probe circuit, (1)(2)
    J. Magn. Reson. 200, 2-5 (2009).
    Abstract
     
  • Takafumi Takahashi, Koji Kanehashi, Yuichi Shimoikeda, Takahiro Nemoto, and Koji Saito
    Practical comparison of sensitivity and resolution between STMAS and MQMAS for 27Al, (1)(2)(3)
    J. Magn. Reson. 198, 228-235 (2009).
    Abstract
     
  • T. J. Ball and S. Wimperis
    Use of SPAM and FAM pulses in high-resolution MAS NMR spectroscopy of quadrupolar nuclei,
    J. Magn. Reson. 187, 343-351 (2007).
     
  • J. W. Wiench, G. Tricot, L. Delevoye, J. Trebosc, J. Frye, L. Montagne, J.-P. Amoureux, and M. Pruski
    SPAM-MQ-HETCOR: an improved method for heteronuclear correlation spectroscopy between quadrupolar and spin-1/2 nuclei in solid-state NMR,
    Phys. Chem. Chem. Phys. 8, 144-150 (2006).
     
  • J.-P. Amoureux, L. Delevoye, G. Fink, F. Taulelle, A. Flambard, and L. Montagne
    Implementing SPAM into STMAS: a net sensitivity improvement in high-resolution NMR of quadrupolar nuclei,
    J. Magn. Reson. 175, 285-299 (2005).
     
  • J.-P. Amoureux, A. Flambard, L. Delevoye, and L. Montagne
    A very sensitive high-resolution NMR method for quadrupolar nuclei: SPAM-DQF-STMAS,
    Chem. Commun.3472-3474 (2005).
     
  • N. Malicki, L. Mafra, A.-A. Quoineaud, J. Rocha, F. Thibault-Starzyk, and C. Fernandez
    Multiplex MQMAS NMR of quadrupolar nuclei, (1)(2)(3)
    Solid State NMR 28, 13-21 (2005).
     
  • Z. H. Gan and H. T. Kwak
    Enhancing MQMAS sensitivity using signals from multiple coherence transfer pathways,
    J. Magn. Reson. 168, 346-351 (2004).
     
 

(top)

[Contact me] - Last updated December 15, 2012
Solid-state NMR bibliography for
Aluminum-27
Antimony-121/123
Arsenic-75
Barium-135/137
Beryllium-9
Bismuth-209
Boron-11
Bromine-79/81
Calcium-43
Cesium-133
Chlorine-35/37
Chromium-53
Cobalt-59
Copper-63/65
Deuterium-2
Gallium-69/71
Germanium-73
Gold-197
Hafnium-177/179
Indium-113/115
Iodine-127
Iridium-191/193
Krypton-83
Lanthanum-139
Lithium-7
Magnesium-25
Manganese-55
Mercury-201
Molybdenum-95/97
Neon-21
Nickel-61
Niobium-93
Nitrogen-14
Osmium-189
Oxygen-17
Palladium-105
Potassium-39/41
Rhenium-185/187
Rubidium-85/87
Ruthenium-99/101
Scandium-45
Sodium-23
Strontium-87
Sulfur-33
Tantalum-181
Titanium-47/49
Vanadium-51
Xenon-131
Zinc-67
Zirconium-91



Copyright 2002- pascal-man.com. All rights reserved.