Reference for MQ-MAS signal enhancement with Quadrupolar CPMG




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MQ-QCPMG-MAS references

Below are provided some NMR references about MQ-MAS with QCPMG sequence applied to half-integer quadrupole spins. These references contain
(1) the pulse-sequence diagram,
(2) the coherence-transfer pathways,
(3) the phase-cycling.

  • F. H. Larsen, S. Rossano, and I. Farnan
    Order and disorder in titanosilicate glass by 17O MAS, off-MAS, and 3Q-QCPMG-MAS solid-state NMR,
    J. Phys. Chem. B 111, 8014-8019 (2007).
     
  • F. H. Larsen and I. Farnan
    Site populations and short range order in aluminosilicates investigated by 27Al solid-state NMR, (1)(2)(3)
    J. Phys. Chem. B 108, 9764-9771 (2004).
     
  • R. Lefort, J. W. Wiench, M. Pruski, and J.-P. Amoureux
    Optimization of data acquisition and processing in Carr-Purcel-Meiboom-Gill MQMAS NMR, (1)(2)
    J. Chem. Phys. 116, 2493-2501 (2002).
     
  • J.-P. Amoureux and M. Pruski
    Advances in MQMAS NMR, (1)(2)
    in Encyclopedia of Nuclear Magnetic Resonance, edited by D. M. Grant and R. K. Harris,
    (J. Wiley, Chichester, Vol. 9, 226-251, 2002).
     
  • L. Frydman
    Fundamentals of MQMAS NMR on half-integer quadrupolar nuclei, (1)(2)
    in Encyclopedia of Nuclear Magnetic Resonance, edited by D. M. Grant and R. K. Harris,
    (J. Wiley, Chichester, Vol. 9, 262-274, 2002).
     
  • F. H. Larsen and N. C. Nielsen
    Effects of finite RF pulses and sample spinning speed in multiple-quantum magic-angle spinning (MQ-MAS) and multiple-quantum quadrupolar Carr-Purcell-Meiboom-Gill magic-angle spinning (MQ-QCPMG-MAS) nuclear magnetic resonance of half-integer, (1)(2)(3)
    J. Phys. Chem. A 103, 10825-10832 (1999).
     
  • T. Vosegaard, F. H. Larsen, H. J. Jakobsen, P. D. Ellis, and N. C. Nielsen
    Sensitivity-enhanced multiple-quantum MAS NMR of half-integer quadrupolar nuclei, (1)(2)
    J. Am. Chem. Soc. 119, 9055-9056 (1997).
     

Related bibliography

  • F. H. Larsen, I. Farnan, and A. S. Lipton
    Separation of 47Ti and 49Ti solid-state NMR lineshapes by static QCPMG experiments at multiple fields,
    J. Magn. Reson. 178, 228-236 (2006).
     
  • C. M. Widdifield and R. W. Schurko
    A solid-state 39K and 13C NMR study of polymeric potassium metallocenes, (1)
    J. Phys. Chem. A 109, 6865-6876 (2005).
     
  • R. Siegel, T. T. Nakashima, and R. E. Wasylishen
    Signal enhancement of NMR spectra of half-integer quadrupolar nuclei in solids using hyperbolic secant pulses, (1)
    Chem. Phys. Lett. 388, 441-445 (2004).
     
  • F. H. Larsen
    Molecular dynamics of half-integer quadrupolar nuclei studied by QCPMG solid-state NMR experiments on static and rotating samples. Theory and simulations,
    J. Magn. Reson. 171, 293-304 (2004).
     
  • G. Mali and V. Kaucic
    Enhancing sensitivity or resolution of homonuclear correlation experiment for half-integer quadrupolar nuclei,
    J. Magn. Reson. 171, 48-56 (2004).
     
  • I. Hung and R. W. Schurko
    Solid-state 91Zr NMR of bis(cyclopentadienyl)dichloro zirconium(IV), (1)
    J. Phys. Chem. B 108, 9060-9069 (2004).
     
  • R. Siegel, T. T. Nakashima, and R. E. Wasylishen
    Application of multiple-pulse experiments to characterize broad NMR chemical-shift powder patterns from spin-1/2 nuclei in the solid state, (1)
    J. Phys. Chem. B 108, 2218-2226 (2004).
     
  • R. W. Schurko, I. Hung, and C. M. Widdifield
    Signal enhancement in NMR spectra of half-integer quadrupolar nuclei via DFS-QCPMG and RAPT-QCPMG pulse sequences, (1)
    Chem. Phys. Lett. 379, 1-10 (2003).
     
  • I. Hung and R. W. Schurko
    Solid-state 25Mg QCPMG NMR of bis(cyclopentadienyl)magnesium,
    Solid State NMR 24, 78-93 (2003).
     
  • M. Bak, J. T. Rasmussen, and N. C. Nielsen
    SIMPSON: A general simulation program for solid-state NMR spectroscopy, (1)
    J. Magn. Reson. 147, 296-330 (2000).
     
  • F. H. Larsen, J. Skibsted, H. J. Jakobsen, and N. C. Nielsen
    Solid-state QCPMG NMR of low-gamma quadrupolar metal nuclei in natural abundance, (1)
    J. Am. Chem. Soc. 122, 7080-7086 (2000).
     
  • F. H. Larsen, H. J. Jakobsen, P. D. Ellis, and N. C. Nielsen
    QCPMG-MAS NMR of half-integer quadrupolar nuclei, (1)
    J. Magn. Reson. 131, 144-147 (1998).
     
  • F. H. Larsen, H. J. Jakobsen, P. D. Ellis, and N. C. Nielsen
    High-field QCPMG-MAS NMR of half-integer quadrupolar nuclei with large quadrupole couplings, (1)
    Mol. Phys. 95, 1185-1195 (1998).
     
  • F. H. Larsen, H. J. Jakobsen, P. D. Ellis, and N. C. Nielsen
    Molecular dynamics from 2H quadrupolar Carr-Purcell-Meiboom-Gill solid-state NMR spectroscopy, (1)(2)
    Chem. Phys. Lett. 292, 467-473 (1998).
     
  • F. H. Larsen, H. J. Jakobsen, P. D. Ellis, and N. C. Nielsen
    Sensitivity-enhanced quadrupolar-echo NMR of half-integer quadrupolar nuclei. Magnitudes and relative orientation of chemical shielding and quadrupolar coupling tensors, (1)(3)
    J. Phys. Chem. A 101, 8597-8606 (1997).
     
 

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[Contact me] - Last updated December 15, 2012
Solid-state NMR bibliography for
Aluminum-27
Antimony-121/123
Arsenic-75
Barium-135/137
Beryllium-9
Bismuth-209
Boron-11
Bromine-79/81
Calcium-43
Cesium-133
Chlorine-35/37
Chromium-53
Cobalt-59
Copper-63/65
Deuterium-2
Gallium-69/71
Germanium-73
Gold-197
Hafnium-177/179
Indium-113/115
Iodine-127
Iridium-191/193
Krypton-83
Lanthanum-139
Lithium-7
Magnesium-25
Manganese-55
Mercury-201
Molybdenum-95/97
Neon-21
Nickel-61
Niobium-93
Nitrogen-14
Osmium-189
Oxygen-17
Palladium-105
Potassium-39/41
Rhenium-185/187
Rubidium-85/87
Ruthenium-99/101
Scandium-45
Sodium-23
Strontium-87
Sulfur-33
Tantalum-181
Titanium-47/49
Vanadium-51
Xenon-131
Zinc-67
Zirconium-91



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