Reference for two-pulse MQ-MAS




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Two-pulse MQ-MAS references

Below are provided some NMR references about MQ-MAS with two-pulse sequence applied to half-integer quadrupole spins. These references contain
(1) the pulse-sequence diagram,
(2) the coherence-transfer pathways,
(3) the phase-cycling.

  • C. M. Morais, M. Lopes, C. Fernandez, and J. Rocha
    Assessing the potential of fast amplitude modulation pulses for improving triple-quantum magic angle spinning NMR spectra of half-integer quadrupolar nuclei, (1)(2)
    Magn. Reson. Chem. 41, 679-688 (2003).
     
  • L. Delevoye, C. Fernandez, C. M. Morais, J.-P. Amoureux, V. Montouillout, and J. Rocha
    Double-resonance decoupling for resolution enhancement of 31P solid-state MAS and 27Al -> 31P MQHETCOR NMR, (1)(2)(3)
    Solid State NMR 22, 501-512 (2002).
     
  • Y. Millot and P. P. Man
    Procedures for labeling the high-resolution axis of two-dimensional MQ-MAS NMR spectra of half-integer quadrupole spins (PDF article, 203 Kb), (1)
    Solid State NMR 21, 21-43 (2002).
     
  • J.-P. Amoureux and M. Pruski
    Advances in MQMAS NMR, (1)(2)
    in Encyclopedia of Nuclear Magnetic Resonance, edited by D. M. Grant and R. K. Harris,
    (J. Wiley, Chichester, Vol. 9, 226-251, 2002).
     
  • L. Frydman
    Fundamentals of MQMAS NMR on half-integer quadrupolar nuclei, (1)(2)
    in Encyclopedia of Nuclear Magnetic Resonance, edited by D. M. Grant and R. K. Harris,
    (J. Wiley, Chichester, Vol. 9, 262-274, 2002).
     
  • A. Goldbourt and P. K. Madhu
    Multiple-Quantum Magic Angle Spinning: High-resolution solid state NMR spectroscopy of half-integer quadrupolar nuclei, (1)(2)(3)
    Monatsh. Chem. 133, 1497-1534 (2002).
     
  • A. Lupulescu, S. P. Brown, and H. W. Spiess
    Rotor-encoded heteronuclear MQ MAS NMR spectroscopy of half-integer quadrupolar and spin I = 1/2 nuclei, (1)
    J. Magn. Reson. 154, 101-129 (2002).
     
  • M. Pruski, J. W. Wiench, and J.-P. Amoureux
    On the conversion of triple- to single-quantum coherences in MQMAS NMR, (1)(2)
    J. Magn. Reson. 147, 286-295 (2000).
     
  • P. K. Madhu, A. Goldbourt, L. Frydman, and S. Vega
    Sensitivity enhancement of the MQMAS NMR experiment by fast amplitude modulation of the pulses, (1)(3)
    Chem. Phys. Lett. 307, 41-47 (1999).
     
  • M. E. Smith and E. R. H. van Eck
    Recent advances in experimental solid state NMR methodology for half-integer spin quadrupolar nuclei, (1)(2)
    Progr. Nucl. Magn. Reson. Spectros. 34, 159-201 (1999).
     
  • A. Medek and L. Frydman
    Multiple-Quantum Magic-Angle Spinning NMR: A new technique for probing quadrupolar nuclei in solids, (1)(2)
    J. Braz. Chem. Soc. 10, 263-277 (1999).
     
  • P. P. Man
    Scaling and labeling the high-resolution isotropic axis of two-dimensional multiple-quantum magic-angle spinning spectra of half-integer quadrupole spins (PDF article, 300 Kb), (1)(2)
    Phys. Rev. B 58, 2764-2782 (1998).
     
  • T. Charpentier, C. Fermon, and J. Virlet
    Numerical and theoretical analysis of multiquantum MAS experiments, (1)(2)
    J. Chem. Phys. 109, 3116-3130 (1998).
     
  • S. Steuernagel
    A new sequence for the MQMAS/HETCOR experiment, (1)(2)
    Solid State NMR 11, 197-201 (1998).
     
  • M. Hanaya and R. K. Harris
    Two-dimensional 23Na MQ MAS NMR study of layered silicates, (1)
    J. Mater. Chem. 8, 1073-1079 (1998).
     
  • S. H. Wang, S. M. De Paul, and L. M. Bull
    High-resolution heteronuclear correlation between quadrupolar and spin-1/2 nuclei using MQ MAS, (1)(2)(3)
    J. Magn. Reson. 125, 364-368 (1997).
     
  • S. P. Brown and S. Wimperis
    Two-dimensional MQ-MAS NMR of quadrupolar nuclei: a comparison of methods, (1)(2)(3)
    J. Magn. Reson. 128, 42-61 (1997).
     
  • S. H. Wang, Z. Xu, J. H. Baltisberger, L. M. Bull, J. F. Stebbins, and A. Pines
    MQ MAS and DAS NMR spectroscopy of quadrupolar nuclei, (1)
    Solid State NMR 8, 1-16 (1997).
     
  • M. Hanaya and R. K. Harris
    Effect of 1H-decoupling in 2D MQ-MAS NMR spectroscopy of 23Na in a hydrous layered silicate, (1)
    Solid State NMR 8, 147-151 (1997).
     
  • M. J. Duer
    Determination of structural data from MQ-MAS NMR experiments, (1)
    Chem. Phys. Lett. 277, 167-174 (1997).
     
  • C. Fernandez, J.-P. Amoureux, L. Delmotte, and H. Kessler
    Crystallographic site probing in the triclinic CHA-like AlPO4 by 27Al 2D quintuple-quantum NMR, (1)(2)(3)
    Microporous Mater. 6, 125-130 (1996).
     
  • C. Fernandez and J.-P. Amoureux
    Triple-quantum MAS NMR of quadrupolar nuclei, (1)(2)
    Solid State NMR 5, 315-321 (1996).
     
  • G. Wu, D. Rovnyak, B. Q. Sun, and R. G. Griffin
    High-resolution multiple quantum MAS NMR spectroscopy of half-integer quadrupolar nuclei, (1)
    Chem. Phys. Lett. 249, 210-217 (1996).
     
  • S. P. Brown, S. J. Heyes, and S. Wimperis
    Two-dimensional MAS multiple-quantum NMR of quadrupolar nuclei. Removal of inhomogeneous second-order broadening, (1)(2)
    J. Magn. Reson. 119, 280-284 (1996).
     
  • D. Massiot, B. Touzo, D. Trumeau, J. P. Coutures, J. Virlet, P. Florian, and P. J. Grandinetti
    Two-dimensional MAS isotropic reconstruction sequences for quadrupolar nuclei, (1)(2)(3)
    Solid State NMR 6, 73-83 (1996).
     
  • A. Medek, J. S. Harwood, and L. Frydman
    Multiple-quantum MAS NMR: a new method for the study of quadrupolar nuclei in solids, (1)(2)(3)
    J. Am. Chem. Soc. 117, 12779-12787 (1995).
     
 

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Niobium-93
Nitrogen-14
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Scandium-45
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Strontium-87
Sulfur-33
Tantalum-181
Titanium-47/49
Vanadium-51
Xenon-131
Zinc-67
Zirconium-91



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