Deuterium-2 NMR

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Isotope Spin Natural
abundance (%)
Quadrupole moment
(10-30m2)
Relative
sensitivity
Absolute
sensitivity
NMR frequency (MHz)
at a field of 2.3488T
Reference
sample
H-1 1/2 99.98 0 1.00 1.00 -100 Me4Si
D-2 1 0.015 0.2860 9.65E-3 1.45E-6 -15.151 (CD3)4Si

Solid-state deuterium NMR references

  1. Adam R. Altenhof, Sungsool Wi, and Robert W. Schurko
    Broadband adiabatic inversion cross-polarization to integer-spin nuclei with application to deuterium NMR,
    Magn. Reson. Chem. 59, 1009-1023 (2021).
    Abstract
  2. Rihards Aleksis, José P. Carvalho, Aleksander Jaworski, and Andrew J. Pell
    Artefact-free broadband 2D NMR for separation of quadrupolar and paramagnetic shift interactions,
    Solid State Nucl. Magn. Reson. 101, 51-61 (2019).
    Abstract
  3. Bryan E. G. Lucier, Yue Zhang, and Yining Huang
    Complete multinuclear solid-state NMR of metal-organic frameworks: The case of α-Mg-formate,
    Concepts Magn. Reson. 45A, 1-19 (2017).
    Free access
  4. Cheng Sun, Xuefeng Wang, and Zhixiao Wang
    Effects of instrumental artifacts on double-quantum-filtered NMR buildup curves for spin I = 1,
    Appl. Magn. Reson. 46, 809-821 (2015).
    Abstract
  5. Ichhuk Karki, Eugene Mihaliuk, and Terry Gullion
    1H-observe 1H-2H dipolar recoupling by REDOR and rotary resonance recoupling,
    Isr. J. Chem. 54, 163-170 (2014).
    Abstract
  6. Mischa Adjei-Acheamfour and Roland Böhmer
    Second-order quadrupole interaction based detection of ultra-slow motions: Tensor operator framework for central-transition spectroscopy and the dynamics in hexagonal ice as an experimental example,
    J. Magn. Reson. 249, 141-149 (2014).
    Abstract
  7. K. J. Mallikarjunaiah, A. Leftin, J. J. Kinnun, M. J. Justice, A. L. Rogozea, H. I. Petrache, and M. F. Brown
    Solid-state 2H NMR shows equivalence of dehydration and osmotic pressures in lipid membrane deformation,
    Biophys. J. 100, 98-107 (2011).
    Abstract
  8. G. Scholz, S. Brehme, R. König, D. Heidemann, and E. Kemnitz
    Crystalline aluminium hydroxide fluorides AlFx(OH)3-x.H2O: Structural insights from 1H and 2H solid state NMR and vibrational spectroscopy,
    J. Phys. Chem. C 114, 10535-10543 (2010).
    Abstract
  9. P. D. Frischmann, G. A. Facey, P. Ghi, A. J. Gallant, D. L. Bryce, F. Lelj, and M. J. MacLachlan
    Capsule formation, carboxylate exchange, and DFT exploration of cadmium cluster metallocavitands: highly dynamic supramolecules,
    J. Am. Chem. Soc. 132, 3893-3908 (2010).
    Abstract
  10. J. F. Zhu, N. Trefiak, T. Woo, and Y. N. Huang
    An investigation of the adsorption of aromatic hydrocarbons in zeolite Na-Y by solid-state NMR spectroscopy,
    Microporous Mesoporous Mater. 114, 474-484 (2008).
  11. G. M. Bowers, D. L. Bish, and R. J. Kirkpatrick
    H2O and cation structure and dynamics in expandable clays: 2H and 39K NMR investigations of hectorite,
    J. Phys. Chem. C 112, 6430-6438 (2008).
  12. C. A. Fyfe, R. J. Darton, C. Schneider, and F. Scheffler
    Solid-state NMR investigation of the possible existence of "Nanoblocks" in the clear solution synthesis of MFI materials,
    J. Phys. Chem. C 112, 80-88 (2008).
  13. M. Mizuno, Y. Suzuki, K. Endo, M. Murakami, M. Tansho, and T. Shimizu
    Molecular dynamics in paramagnetic materials as studied by magic-angle spinning 2H NMR spectra,
    J. Phys. Chem. A 111, 12954-12960 (2007).
  14. E. S. Mananga, R. Roopchand, Y. S. Rumala, and G. S. Boutis
    On the application of magic echo cycles for quadrupolar echo spectroscopy of spin-1 nuclei,
    J. Magn. Reson. 185, 28-37 (2007).
  15. C. Odin
    NMR studies of phase transitions,
    Annu. Rep. Nucl. Magn. Reson. Spectrosc. 59, 117-205 (2006).
  16. M. Cutajar, S. E. Ashbrook, and S. Wimperis
    2H double-quantum MAS NMR spectroscopy as a probe of dynamics on the microsecond timescale in solids,
    Chem. Phys. Lett. 423, 276-281 (2006).
  17. Y. Y. Huang, R. L. Vold, and G. L. Hoatson
    Investigation of multiaxis molecular motion by off-magic angle spinning deuteron NMR,
    J. Chem. Phys. 124, 104504/1-104504/14 (2006).
  18. E. S. Mananga, Y. S. Rumala, and G. S. Boutis
    Finite pulse width artifact suppression in spin-1 quadrupolar echo spectra by phase cycling,
    J. Magn. Reson. 181, 296-303 (2006).
  19. Eric Hughes, Jason Jordan, and Terry Gullion
    Structural characterization of the [Cs(p-tert-butylcalix[4]arene-H)(MeCN)] guest-host system by 13C-133Cs REDOR NMR,
    J. Phys. Chem. B 105, 5887-5891 (2001).
    Abstract
  20. T. Bräuniger, R. Poupko, Z. Luz, D. Reichert, H. Zimmermann, H. Schmitt, and U. Haeberlen
    Orientational disorder in 1,2,3-trichloro-4,5,6-trimethylbenzene. A single crystal deuterium NMR study of the site populations and dynamics,
    Phys. Chem. Chem. Phys. 3, 1891-1903 (2001).
    Abstract
  21. T. Bräuniger, R. Poupko, Z. Luz, H. Zimmermann, and U. Haeberlen
    Quantification of the orientational disorder in ortho-dichlorotetramethylbenzene: A single crystal deuterium nuclear magnetic resonance and x-ray study of the site populations,
    J. Chem. Phys. 115, 8049-8059 (2001).
    Abstract
  22. T. Bräuniger, R. Poupko, Z. Luz, P. Gutsche, C. Meinel, H. Zimmermann, and U. Haeberlen
    The dynamic disorder of azulene: A single crystal deuterium nuclear magnetic resonance study,
    J. Chem. Phys. 112, 10858-10870 (2000).
    Abstract
  23. A. Detken and H. Zimmermann
    Reorientational tunneling of partially deuterated methyl groups: A single-crystal deuteron NMR study of aspirin-CH2D,
    J. Chem. Phys. 108, 5845-5854 (1998).
    Abstract
  24. P. Speier, H. Zimmermann, U. Haeberlen, and Z. Luz
    Dynamic disorder in 2,3-dimethylnaphthalene: a single crystal deuteron nuclear magnetic resonance study,
    Mol. Phys. 95, 1153-1167 (1998).
    Abstract
  25. B. Tesche, H. Zimmermann, R. Poupko, and U. Haeberlen
    The single-rotation method of determining quadrupole coupling tensors in monoclinic crystals. Error analysis and application to bullvalene,
    J. Magn. Reson. A 104, 68-77 (1993).
    Abstract
  26. H. Eckert, J. P. Yesinowski, and E. M. Stolper
    Quantitative NMR studies of water in silicate glasses,
    Solid State Ionics 32/33, 298-313 (1989).
  27. N. J. Heaton, R. R. Vold, and R. L. Vold
    Deuterium quadrupole-echo NMR spectroscopy. IV. Inversion of full width deuterium powder patterns,
    J. Magn. Reson. 77, 572-576 (1988).
    Abstract
  28. H. Eckert, J. P. Yesinowski, E. M. Stolper, T. R. Stanton, and J. Holloway
    The state of water in rhyolitic glasses: a deuterium NMR study,
    J. Non-Cryst. Solids 93, 93-114 (1987).
  29. M. S. Greenfield, A. D. Ronemus, R. L. Vold, R. R. Vold, P. D. Ellis, and T. E. Raidy
    Deuterium quadrupole-echo NMR spectroscopy. III. Practical aspects of lineshape calculations for multiaxis rotational processes,
    J. Magn. Reson. 72, 89-103 (1987).
    Abstract
  30. A. D. Ronemus, R. L. Vold, and R. R. Vold
    Deuterium quadrupole-echo NMR spectroscopy. II. Artifact suppression,
    J. Magn. Reson. 70, 416-426 (1986).
    Abstract
  31. T. M. Barbara, M. S. Greenfield, R. L. Vold, and R. R. Vold
    Deuterium quadrupole-echo NMR spectroscopy. I. Effects of chemical exchange during single and composite pulses,
    J. Magn. Reson. 69, 311-330 (1986).
    Abstract
  32. D. J Siminovitch and R. G Griffin
    Finite pulse-width effects in inversion-recovery experiments on I = 1 nuclei,
    J. Magn. Reson. 62, 99-108 (1985).
    Abstract
  33. Myer Bloom, James H. Davis, and Marko I. Valic
    Spectral distortion effects due to finite pulse widths in deuterium nuclear magnetic resonance spectroscopy,
    Can. J. Phys. 58, 1510-1517 (1980).
    Abstract
  34. R. Hentschel and H. W. Spiess
    Deuterium Fourier transform NMR in solids and solid polymers,
    J. Magn. Reson. 35, 157-162 (1979).
    Abstract
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