TopSpin 2.1, Avance III:
MQMAS for half-integer quadrupole spin




Home and Applets > Pulse Program > TopSpin 2.1, Avance III > MQMAS for Half-Integer Quadrupole Spin

Amplitude-modulated MQMAS experiments:


  • Z-filter
    The same pulse program as that defined for XWINNMR 3.5 operating system
  • SPAM-echo/antiecho (2D only)
    The only change is the addtion of 3u delay before the two signal storage lines in the pulse program for XWINNMR 3.5 operating system
  • MQMAS data processing:
    Shearing the 2D spectrum with AU program xfshear



Phase-modulated MQMAS experiments:


  • Multiplex SPAM (2D only)
    The same pulse program as that defined for XWINNMR 3.5 operating system
  • The AU program MSM (Multiplex SPAM MQ) remains valid

  1. Advanced Quadrupolar NMR (6 Mb PDF file) by Sharon Ashbrook, School of Chemistry, University of St Andrews
  2. High-resolution solid-state NMR of quadrupolar nuclei, tutorial lecture presented at the Bruker user's meeting Breckenridge, Colorado July 2007 (25 Mb PDF file) by Philip J. Grandinetti, Ohio State University
  3. Applications of nuclear magnetic resonance to metal hydrogen materials, Summer School Lectures presented at MH2008 23 June 2008 (5 Mb PDF file) by Son-Jong Hwang and Robert C. Bowman, Jr. California Institute of Technology, Pasadena
  4. High-field solid-state NMR: The tools and their application in materials research, Lectures presented at the International School on "MAGNETIC FIELDS FOR SCIENCE", Cargèse, Corsica, France, August 27th - September 8th, 2007 (10 Mb PDF file) by Arno Kentgens Department of Physical Chemistry / solid-state NMR, Institute for Molecules and Materials, Radboud University Nijmegen, The Netherlands
 

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Solid-state NMR bibliography for
Aluminum-27
Antimony-121/123
Arsenic-75
Barium-135/137
Beryllium-9
Bismuth-209
Boron-11
Bromine-79/81
Calcium-43
Cesium-133
Chlorine-35/37
Chromium-53
Cobalt-59
Copper-63/65
Deuterium-2
Gallium-69/71
Germanium-73
Gold-197
Hafnium-177/179
Indium-113/115
Iodine-127
Iridium-191/193
Krypton-83
Lanthanum-139
Lithium-7
Magnesium-25
Manganese-55
Mercury-201
Molybdenum-95/97
Neon-21
Nickel-61
Niobium-93
Nitrogen-14
Osmium-189
Oxygen-17
Palladium-105
Potassium-39/41
Rhenium-185/187
Rubidium-85/87
Ruthenium-99/101
Scandium-45
Sodium-23
Strontium-87
Sulfur-33
Tantalum-181
Titanium-47/49
Vanadium-51
Xenon-131
Zinc-67
Zirconium-91



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