TopSpin 2.1, Avance III:
2Q/1Q correlation




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Double-quantum/single-quantum correlation experiments:


cnst31: sample rotation frequency

----------------------------

  • B1=7*cnst31
  • pc71d: 1D POST_C7 double-quantum excitation.
  • pc72d: 2D POST_C7 double-quantum excitation, t1 increment in0 = n/cnst31.
  • pc72dlsw: 2D large double-quantum F1 spectral width POST_C7 excitation, t1 increment inf1 = n(2/cnst31)/7.
  • pc72dbigsw: 2D big double-quantum F1 spectral width POST_C7 excitation, t1 increment inf1 = p9.
    ----------------------------
  • pc7cp2d: 2D cross-polarization POST_C7 double-quantum excitation, t1 increment in0 = n/cnst31.

  • B1=7*cnst31
  • r14-2-6_1d: 1D R1426 double-quantum excitation.
  • r14-2-6_2d: 2D R1426 double-quantum excitation, t1 increment in0 = n/cnst31.
  • r14-2-6_2dbsw: 2D big double-quantum F1 spectral width R1426 excitation, t1 increment inf1 = p9.
    ----------------------------
  • r14-2-6hp_2d: 2D high-power decoupling for R1426 double-quantum excitation, t1 increment in0 = n/cnst31.

  • B1=5*cnst31
  • spc51d: 1D SPC5 double-quantum excitation.
  • spc52d: 2D SPC5 double-quantum excitation, t1 increment in0 = n/cnst31.
  • spc52dlsw: 2D large double-quantum F1 spectral width SPC5 excitation, t1 increment inf1 = n(2/cnst31)/5.
  • spc52dbigsw: 2D big double-quantum F1 spectral width SPC5 excitation, t1 increment inf1 = p9.
    ----------------------------
  • spc5cp1d: 1D cross polarization for SPC5 double-quantum excitation.
  • spc5cp2d: 2D cross polarization for SPC5 double-quantum excitation, t1 increment in0 = n/cnst31.
  • spc5cp2dlsw: 2D cross polarization for large double-quantum F1 spectral width SPC5 excitation, t1 increment inf1 = n(2/cnst31)/5.
  • spc5cp2dbigsw: 2D cross polarization for big double-quantum F1 spectral width SPC5 excitation, t1 increment inf1 = p9.

  • B1=3.5*cnst31
  • c14-4-5_1d: 1D C1445 double-quantum excitation.
  • c14-4-5_2dbsw: 2D big double-quantum F1 spectral width C1445 excitation, t1 increment inf1 = p9.
    ----------------------------
  • c14-4--5_1d: 1D C144-5 double-quantum excitation.

  • B1=3*cnst31
  • r12-2-5_1d: 1D R1225 double-quantum excitation.
  • r12-2-5_2d: 2D R1225 double-quantum excitation, t1 increment in0 = n/cnst31.
  • r12-2-5_2dbsw: 2D big double-quantum F1 spectral width R1225 excitation, t1 increment inf1 = p9.

  • B1=1.75*cnst31
  • r14-4-5_1d: 1D R1445 double-quantum excitation.
  • r14-4-5_2d: 2D R1445 double-quantum excitation, t1 increment in0 = n/cnst31.
  • r14-4-5_2dbsw: 2D big double-quantum F1 spectral width R1445 excitation, t1 increment inf1 = p9.

  • B1 and cnst31 are independent
  • baba1: 1D/2D HP decoupling 1-rotor period BABA double-quantum excitation.
  • baba2rot: 1D/2D 2-rotor period BABA double-quantum excitation.
  • babacp2: 1D/2D cross polarization for 2-rotor period BABA double-quantum excitation.

  1. Using symmetry to design pulse sequences in solid-state NMR, Leiden-SSNMR-2000 (0.5 Mb PDF file) by Malcolm Levitt, Stockholm University, Sweden
  2. Deanne Marie Taylor,
    "Nuclear Magnetic Resonance Coherence Transfer in a Homonuclear Two Spin-1/2 Solid-State System." Biophysics Graduate Program, University of Michigan 2001.
    Dissertation
 

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Solid-state NMR bibliography for
Aluminum-27
Antimony-121/123
Arsenic-75
Barium-135/137
Beryllium-9
Bismuth-209
Boron-11
Bromine-79/81
Calcium-43
Cesium-133
Chlorine-35/37
Chromium-53
Cobalt-59
Copper-63/65
Deuterium-2
Gallium-69/71
Germanium-73
Gold-197
Hafnium-177/179
Indium-113/115
Iodine-127
Iridium-191/193
Krypton-83
Lanthanum-139
Lithium-7
Magnesium-25
Manganese-55
Mercury-201
Molybdenum-95/97
Neon-21
Nickel-61
Niobium-93
Nitrogen-14
Osmium-189
Oxygen-17
Palladium-105
Potassium-39/41
Rhenium-185/187
Rubidium-85/87
Ruthenium-99/101
Scandium-45
Sodium-23
Strontium-87
Sulfur-33
Tantalum-181
Titanium-47/49
Vanadium-51
Xenon-131
Zinc-67
Zirconium-91



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