Nutation NMR pulse programs for Avance spectrometers with XwinNMR 3.5 operating system




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AVANCE spectrometers
with xwinnmr 3.5 operating system

SF = BF1 + SR (Larmor frequency of reference sample)

SFO1 = BF1 + O1 (spectrometer frequency)

These pulse programs are available for both 1D and 2D NMR experiments.

amplitude-modulated
experiments:






phase-modulated
experiments:







1-dimensional experiments:


  • qcpmgall.av, pulse program which samples continuously, including ALL pulses and ringdown delays
  • au_qcpmg, AU program which takes out data points sampled during pulses and ring down delays.
    If digmod is used, convert data to analog with convdta command.
    ALWAYS use this AU program on a COPY of dataset.
  • qcpmgaddjt from Julien Trébosc, AU program which stores echos from qcpmgall.av pulse program by adding them up.
    Use absolute scale for Y-axis to check the amplitude of echo in the FID window.
    If digmod is used, convert data to analog with convdta command.
    ALWAYS use this AU program on a COPY of dataset.
  • qcpmgsplit, AU program for splitting CPMG echo train acquired with qcpmgall.av pulse program. These echoes allow T2 measurement.

  • hpdecqcpmgall.av, pulse program for performing CPMG experiment with high power decoupling , which samples continuously, including ALL pulses and ringdown delays
  • cpqcpmgall.av, pulse program for performing basic cross-polarisation experiment with CPMG detection, which samples continuously, including ALL pulses and ringdown delays


AVANCE hardware

Acquisition commands and parameters

Processing commands and parameters

Au programming

Avance I Solid State NMR by Jochem Struppe

Z-filtered STMAS pulse program

One pulse program with digital phase for the receiver

Bruker NMR guide, version 3.5

Bruker NMR guide, version 3.0

Iowa State University - Mei Hong research group

 

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[Contact me] - Last updated February 07, 2013
Solid-state NMR bibliography for
Aluminum-27
Antimony-121/123
Arsenic-75
Barium-135/137
Beryllium-9
Bismuth-209
Boron-11
Bromine-79/81
Calcium-43
Cesium-133
Chlorine-35/37
Chromium-53
Cobalt-59
Copper-63/65
Deuterium-2
Gallium-69/71
Germanium-73
Gold-197
Hafnium-177/179
Indium-113/115
Iodine-127
Iridium-191/193
Krypton-83
Lanthanum-139
Lithium-7
Magnesium-25
Manganese-55
Mercury-201
Molybdenum-95/97
Neon-21
Nickel-61
Niobium-93
Nitrogen-14
Osmium-189
Oxygen-17
Palladium-105
Potassium-39/41
Rhenium-185/187
Rubidium-85/87
Ruthenium-99/101
Scandium-45
Sodium-23
Strontium-87
Sulfur-33
Tantalum-181
Titanium-47/49
Vanadium-51
Xenon-131
Zinc-67
Zirconium-91



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