NMR pulse sequence:
ST-MAS
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衛星躍遷魔角旋轉




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Satellite Transition Magic Angle Spinning references

Below are provided some NMR references about ST-MAS applied to half-integer quadrupole spins. These references contain
(1) the pulse-sequence diagram,
(2) the coherence-transfer pathways,
(3) the phase-cycling,
(4) the receiver-phase relationship.

  • Takafumi Takahashi, Shunsuke Kashiwakura, Koji Kanehashi, and Tetsuya Nagasaka
    First high-resolution 11B nuclear magnetic resonance (NMR) spectra of coal fly ash by satellite-transition magic angle spinning (STMAS) NMR, (1)(2)
    Energy Fuels 23, 1778-1780 (2009).
    Abstract
     
  • Takafumi Takahashi, Koji Kanehashi, Yuichi Shimoikeda, Takahiro Nemoto, and Koji Saito
    Practical comparison of sensitivity and resolution between STMAS and MQMAS for 27Al, (1)(2)(3)
    J. Magn. Reson. 198, 228-235 (2009).
    Abstract
     
  • J. Trebosc, J.-P. Amoureux, and Z. H. Gan
    Comparison of high-resolution solid-state NMR MQMAS and STMAS methods for half-integer quadrupolar nuclei, (1)
    Solid State NMR 31, 1-9 (2007).
     
  • J.-P. Amoureux and J. Trébosc
    Homogeneous broadenings in 2D solid-state NMR of half-integer quadrupolar nuclei, (1)(2)
    J. Magn. Reson. 179, 311-316 (2006).
     
  • O. B. Lapina, D. F. Khabibulin, K. V. Romanenko, Z. H. Gan, M. G. Zuev, V. N. Krasil'nikov, and V. E. Fedorov
    93Nb NMR chemical shift scale for niobia systems,
    Solid State NMR 28, 204-224 (2005).
     
  • J.-P. Amoureux, A. Flambard, L. Delevoye, and L. Montagne
    A very sensitive high-resolution NMR method for quadrupolar nuclei: SPAM-DQF-STMAS, (1)(2)
    Chem. Commun.3472-3474 (2005).
     
  • J.-P. Amoureux, L. Delevoye, G. Fink, F. Taulelle, A. Flambard, and L. Montagne
    Implementing SPAM into STMAS: a net sensitivity improvement in high-resolution NMR of quadrupolar nuclei, (1)(2)(3)
    J. Magn. Reson. 175, 285-299 (2005).
     
  • Sharon E. Ashbrook and Stephen Wimperis,
    High-resolution NMR of quadrupolar nuclei in solids: the satellite-transition magic angle spinning (STMAS) experiment, (1)(2)(3)
    Progr. Nucl. Magn. Reson. Spectrosc. 45, 53-108 (2004).
     
  • N. G. Dowell, S. E. Ashbrook, and S. Wimperis
    Satellite-transition MAS NMR of low-gamma nuclei at natural abundance: sensitivity, practical implementation, and application to 39K (I = 3/2) and 25Mg (I = 5/2), (1)(2)
    J. Phys. Chem. B 108, 13292-13299 (2004).
     
  • Z. Gan, P. Srinivasan, J. R. Quine, S. Steuernagel, and B. Knott
    Third-order effect in solid-state NMR of quadrupolar nuclei,
    Chem. Phys. Lett. 367, 163-169 (2003).
     
  • J.-P. Amoureux, C. Morais, J. Trebosc, J. Rocha, and C. Fernandez
    I-STMAS, a new high-resolution solid-state NMR method for half-integer, (1)(2)(3)
    Solid State NMR 23, 213-223 (2003).
     
  • S. Wi, S. E. Ashbrook, S. Wimperis, L. Frydman
    Second-order quadrupole-shielding effects in magic-angle spinning solid-state nuclear magnetic resonance,
    J. Chem. Phys. 118, 3131-3140 (2003).
     
  • H. T. Kwak and Z. H. Gan
    Double-quantum filtered STMAS, (1)(2)(3)
    J. Magn. Reson. 164, 369-372 (2003).
     
  • S. E. Ashbrook and S. Wimperis
    SCAM-STMAS: satellite-transition MAS NMR of quadrupolar nuclei with self-compensation for magic-angle misset, (1)(2)(3)
    J. Magn. Reson. 162, 402-416 (2003).
     
  • J.-P. Amoureux, C. Huguenard, F. Engelke, and F. Taulelle
    Unified representation of MQMAS and STMAS NMR of half-integer quadrupolar nuclei,
    Chem. Phys. Lett. 356, 497-504 (2002).
     
  • S. E. Ashbrook and S. Wimperis
    Satellite-transition MAS NMR of spin I = 3/2, 5/2, 7/2, and 9/2 nuclei: sensitivity, resolution, and practical implementation, (1)(2)(3)
    J. Magn. Reson. 156, 269-281 (2002).
     
  • C. Huguenard, F. Taulelle, B. Knott, and Z. Gan
    Optimizing STMAS, (1)(2)(3)
    J. Magn. Reson. 156, 131-137 (2002).
     
  • S. E. Ashbrook and S. Wimperis
    High-resolution NMR spectroscopy of quadrupolar nuclei in solids: satellite-transition MAS with self-compensation for magic-angle misset, (1)(2)(3)
    J. Am. Chem. Soc. 124, 11602-11603 (2002).
     
  • Z. Gan, P. Gor'kov, T. A. Cross, A. Samoson, and D. Massiot
    Seeking higher resolution and sensitivity for NMR of quadrupolar nuclei at ultrahigh magnetic fields,
    J. Am. Chem. Soc. 124, 5634-5635 (2002).
     
  • K. J. Pike, S. E. Ashbrook, and S. Wimperis
    Two-dimensional satellite-transition MAS NMR of quadrupolar nuclei: shifted echoes, high-spin nuclei and resolution, (1)(2)(3)
    Chem. Phys. Lett. 345, 400-408 (2001).
     
  • Z. Gan
    Satellite transition magic-angle spinning nuclear magnetic resonance of half-integer quadrupolar nuclei, (1)(2)(3)
    J. Chem. Phys. 114, 10845-10853 (2001).
     
  • Z. Gan
    Isotopic NMR spectra of half-integer quadrupolar nuclei using satellite transitions and magic-angle spinning, (3)
    J. Am. Chem. Soc. 122, 3242-3243 (2000).
     
 

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[Contact me] - Last updated December 15, 2012
Solid-state NMR bibliography for
Aluminum-27
Antimony-121/123
Arsenic-75
Barium-135/137
Beryllium-9
Bismuth-209
Boron-11
Bromine-79/81
Calcium-43
Cesium-133
Chlorine-35/37
Chromium-53
Cobalt-59
Copper-63/65
Deuterium-2
Gallium-69/71
Germanium-73
Gold-197
Hafnium-177/179
Indium-113/115
Iodine-127
Iridium-191/193
Krypton-83
Lanthanum-139
Lithium-7
Magnesium-25
Manganese-55
Mercury-201
Molybdenum-95/97
Neon-21
Nickel-61
Niobium-93
Nitrogen-14
Osmium-189
Oxygen-17
Palladium-105
Potassium-39/41
Rhenium-185/187
Rubidium-85/87
Ruthenium-99/101
Scandium-45
Sodium-23
Strontium-87
Sulfur-33
Tantalum-181
Titanium-47/49
Vanadium-51
Xenon-131
Zinc-67
Zirconium-91



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