Reference for RIACT MQ-MAS




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RIACT MQ-MAS references

Below are provided some NMR references about MQ-MAS with Rotation Induced Adiabatic Coherence Transfer sequence applied to half-integer quadrupole spins. These references contain
(1) the pulse-sequence diagram,
(2) the coherence-transfer pathways,
(3) the phase-cycling,
(4) the receiver phase relationship.

  • David Rovnyak and Paul E. Kennedy
    Application of shaped adiabatic pulses to MQMAS NMR spectroscopy of spin 3/2 nuclei, (1)
    J. Magn. Reson. 196, 191-199 (2009).
    Abstract
     
  • Renée Siegel, T. T. Nakashima, and R. E. Wasylishen
    Sensitivity enhancement of MQMAS NMR spectra of spin 3/2 nuclei using hyperbolic secant pulses, (1)(2)
    Chem. Phys. Lett. 403, 353-358 (2005).
     
  • H.-T. Kwak, S. Prasad, T. Clark, and P. J. Grandinetti
    Selective suppression and excitation of solid-state NMR resonances based on quadrupole coupling constants, (1)(2)(4)
    J. Magn. Reson. 160, 107-113 (2003).
     
  • A. Jerschow and R. Kumar
    Calculation of coherence pathway selection and cogwheel cycles, (1)(2)
    J. Magn. Reson. 160, 59-64 (2003).
     
  • M. H. Levitt, P. K. Madhu, and C. E. Hughes
    Cogwheel phase cycling, (1)(2)(3)
    J. Magn. Reson. 155, 300-306 (2002).
     
  • P. K. Madhu and M. H. Levitt
    Signal enhancement in the triple-quantum magic-angle spinning NMR of spins-3/2 in solids: the FAM--RIACT--FAM sequence,
    J. Magn. Reson. 155, 150-155 (2002).
     
  • A. Goldbourt and P. K. Madhu
    Multiple-Quantum Magic Angle Spinning: High-resolution solid state NMR spectroscopy of half-integer quadrupolar nuclei, (1)(2)
    Monatsh. Chem. 133, 1497-1534 (2002).
     
  • K. H. Lim, T. Charpentier, and A. Pines
    Efficient triple-quantum excitation in modified RIACT MQMAS NMR for I = 3/2 nuclei, (1)(2)
    J. Magn. Reson. 154, 196-204 (2002).
     
  • L. Frydman
    Fundamentals of MQMAS NMR on half-integer quadrupolar nuclei, (1)(2)
    in Encyclopedia of Nuclear Magnetic Resonance, edited by D. M. Grant and R. K. Harris,
    (J. Wiley, Chichester, Vol. 9, 262-274, 2002).
     
  • H.-T. Kwak, S. Prasad, Y. Yao, P. J. Grandinetti, J. R. Sachleben, and L. Emsley
    Enhanced sensitivity in RIACT/MQ-MAS NMR experiments using rotor assisted population transfer, (1)(2)(3)
    J. Magn. Reson. 150, 71-80 (2001).
    Erratum: J. Magn. Reson. 153, 151-154 (2001).
     
  • A. Goldbourt, P. K. Madhu, S. Kababya, and S. Vega
    The influence of the radiofrequency excitation and conversion pulses on the lineshapes and intensities of the triple-quantum MAS NMR spectra of I = 3/2 nuclei, (1)
    Solid State NMR 18, 1-16 (2000).
     
  • M. E. Smith and E. R. H. van Eck
    Recent advances in experimental solid state NMR methodology for half-integer spin quadrupolar nuclei, (1)(2)
    Progr. Nucl. Magn. Reson. Spectros. 34, 159-201 (1999).
     
  • T. Mildner, M. E. Smith, and R. Dupree
    2D five quantum MAS NMR using rotationally induced coherence transfer, (3)
    Chem. Phys. Lett. 306, 297-302 (1999).
     
  • T. Mildner, M. E. Smith, and R. Dupree
    Rotationally induced triple quantum coherence excitation in MAS NMR spectroscopy of I = 5/2 spins, (1)(3)
    Chem. Phys. Lett. 301, 389-394 (1999).
     
  • K. H. Lim and C. P. Grey
    Analysis of the anisotropic dimension in the RIACT (II) MQ-MAS NMR experiment for I = 3/2 nuclei, (1)(3)
    Solid State NMR 13, 101-112 (1998).
     
  • G. Wu, D. Rovnyak, and R. G. Griffin
    Quantitative multiple-quantum MAS NMR spectroscopy of quadrupolar nuclei in solids, (1)(3)
    J. Am. Chem. Soc. 118, 9326-9332 (1996).
     

Related bibliography

  • S. Caldarelli, A. Buchholz, and M. Hunger
    Investigation of sodium cations in hydrated zeolites LSX, X, and Y by 23Na off-resonance RIACT triple- quantum and high-speed MAS NMR spectroscopy,
    J. Am. Chem. Soc. 123, 7118-7123 (2001).
     
  • S. Caldarelli and F. Ziarelli
    Spectral editing of solid-state MAS NMR spectra of half-integer quadrupolar nuclei,
    J. Am. Chem. Soc. 122, 12015-12016 (2000).
     
  • T. Charpentier, C. Fermon, and J. Virlet
    Efficient time propagation technique for MAS NMR simulation: Application to quadrupolar nuclei,
    J. Magn. Reson. 132, 181-190 (1998).
     
  • A. J. Vega
    MAS NMR spin locking of half-integer quadrupolar nuclei,
    J. Magn. Reson. 96, 50-68 (1992).
     
 

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Nickel-61
Niobium-93
Nitrogen-14
Osmium-189
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Palladium-105
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Rubidium-85/87
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Scandium-45
Sodium-23
Strontium-87
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Titanium-47/49
Vanadium-51
Xenon-131
Zinc-67
Zirconium-91



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