Reference for shifted-echo MQ-MAS




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Shifted-echo MQ-MAS references

Below are provided some NMR references about MQ-MAS with shifted-echo pulse sequence applied to half-integer quadrupole spins. These references contain
(1) the pulse-sequence diagram,
(2) the coherence-transfer pathways,
(3) the phase-cycling,
(4) the receiver-phase relationship.

  • K. H. Lim, T. Charpentier, and A. Pines
    Efficient triple-quantum excitation in modified RIACT MQMAS NMR for I = 3/2 nuclei, (1)(2)
    J. Magn. Reson. 154, 196-204 (2002).
     
  • J.-P. Amoureux and M. Pruski
    Advances in MQMAS NMR, (1)(2)
    in Encyclopedia of Nuclear Magnetic Resonance, edited by D. M. Grant and R. K. Harris,
    (J. Wiley, Chichester, Vol. 9, 226-251, 2002).
     
  • L. Frydman
    Fundamentals of MQMAS NMR on half-integer quadrupolar nuclei, (1)(2)
    in Encyclopedia of Nuclear Magnetic Resonance, edited by D. M. Grant and R. K. Harris,
    (J. Wiley, Chichester, Vol. 9, 262-274, 2002).
     
  • P. D. Zhao, P. S. Neuhoff, and J. F. Stebbins
    Comparison of FAM mixing to single-pulse mixing in 17O 3Q- and 5Q-MAS NMR of oxygen sites in zeolites, (1)(2)
    Chem. Phys. Lett. 344, 325-332 (2001).
     
  • H.-T. Kwak, S. Prasad, Y. Yao, P. J. Grandinetti, J. R. Sachleben, and L. Emsley
    Enhanced sensitivity in RIACT/MQ-MAS NMR experiments using rotor assisted population transfer, (1)(2)
    J. Magn. Reson. 150, 71-80 (2001).
     
  • S. Prasad, P. Zhao, J. Huang, J. J. Fitzgerald, and J. S. Shore
    Niobium-93 MQMAS NMR spectroscopy study of alkali and lead niobates, (1)(4)
    Solid State NMR 19, 45-62 (2001).
     
  • T. Vosegaard, D. Massiot, and P. J. Grandinetti
    Sensitivity enhancements in MQ-MAS NMR of spin-5/2 nuclei using modulated RF mixing pulses, (1)(2)(3)
    Chem. Phys. Lett. 326, 454-460 (2000).
     
  • T. Charpentier, C. Fermon, and J. Virlet
    Numerical and theoretical analysis of multiquantum MAS experiments, (1)(2)
    J. Chem. Phys. 109, 3116-3130 (1998).
     
  • S. P. Brown and S. Wimperis
    Two-dimensional MQ-MAS NMR of quadrupolar nuclei: a comparison of methods, (1)(2)(3)
    J. Magn. Reson. 128, 42-61 (1997).
     
  • S. H. Wang, Z. Xu, J. H. Baltisberger, L. M. Bull, J. F. Stebbins, and A. Pines
    MQ MAS and DAS NMR spectroscopy of quadrupolar nuclei, (1)
    Solid State NMR 8, 1-16 (1997).
     
  • J. H. Baltisberger, Z. Xu, J. F. Stebbins, S. H. Wang, and A. Pines
    Triple-quantum 2D 27Al MAS NMR spectroscopy study of aluminosilicate and aluminate crystals and glasses, (1)(2)
    J. Am. Chem. Soc. 118, 7209-7214 (1996).
     
  • D. Massiot, B. Touzo, D. Trumeau, J. P. Coutures, J. Virlet, P. Florian, and P. J. Grandinetti
    Two-dimensional MAS isotropic reconstruction sequences for quadrupolar nuclei, (1)(2)(3)
    Solid State NMR 6, 73-83 (1996).
     

Related bibliography

  • P. J. Grandinetti, J. H. Baltisberger, A. Llor, Y. K. Lee, U. Werner, M. A. Eastman, and A. Pines
    Pure-absorption-mode lineshapes and sensitivity in two-dimensional DAS NMR,
    J. Magn. Reson. A 103, 72-81 (1993).
     
 

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