NMR pulse sequence:
spin-locking




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Spin-locking-MAS

Some NMR references about spin-locking pulse sequences applied to half-integer quadrupole spins:

  • Sharon E. Ashbrook and Stephen Wimperis
    Spin-locking of half-integer quadrupolar nuclei in nuclear magnetic resonance of solids: Second-order quadrupolar and resonance offset effects,
    J. Chem. Phys. 131, 194509/1-194509/15 (2009).
    Abstract
     
  • G. Mali
    Spin-locking and recoupling of homonuclear dipolar interaction between spin-3/2 nuclei under magic-angle sample spinning,
    J. Magn. Reson. 185, 318-325 (2007).
     
  • S. P. Puls and H. Eckert
    Site discrimination in mixed-alkali glasses studied by cross-polarization NMR,
    J. Phys. Chem. B 110, 14253-14261 (2006).
     
  • S. E. Ashbrook and S. Wimperis
    Spin-locking of half-integer quadrupolar nuclei in nuclear magnetic resonance of solids: Creation and evolution of coherences,
    J. Chem. Phys. 120, 2719-2731 (2004).
     
  • S. Wi, J. W. Logan, D. Sakellariou, J. D. Walls, and A. Pines
    Rotary resonance recoupling for half-integer quadrupolar nuclei in solid-state nuclear magnetic resonance spectroscopy,
    J. Chem. Phys. 117, 7024-7033 (2002).
     
  • M. Baldus, D. Rovnyak, and R. G. Griffin
    Radio-frequency-mediated dipolar recoupling among half-integer quadrupolar spins,
    J. Chem. Phys. 112, 5902-5909 (2000).
     
  • Y. Zhang, F. Deng, J. Qiu, and C. Ye
    Spin-locking mechanism of spin I = 3/2 quadrupolar nuclei undergo magic angle spinning,
    Solid State NMR 15, 209-216 (2000).
     
  • Gunnar Jeschke
    Spin locking of I = 3/2 nuclei in static and spinning samples: A description by abstract spins and Floquet formalism,
    J. Chem. Phys. 108, 907-917 (1998).
     
  • L. van Wüllen, L. Züchner, W. Müller-Warmuth, and H. Eckert
    11B{27Al} and 27Al{11B} double resonance experiments on a glassy sodium aluminoborate,
    Solid State NMR 6, 203-212 (1996).
     
  • W. Sun, J. T. Stephen, L. D. Potter, and Y. Wu
    Rotation-induced resonance and second-order quadrupolar effects on spin locking of half-integer quadrupolar nuclei,
    J. Magn. Reson. A 116, 181-188 (1995).
     
  • S. Ding and C. A. McDowell
    Spin-locking spectral lineshapes of the central transition of half-integer quadrupole systems under MAS,
    J. Molec. Struct. 355, 135-142 (1995).
     
  • S. Hayashi
    MAS NMR of half-integer quadrupole nuclei: effect of spin-locking efficiency on powder lineshapes,
    Solid State NMR 3, 93-101 (1994).
     
  • A. J. Vega
    MAS NMR spin locking of half-integer quadrupolar nuclei,
    J. Magn. Reson. 96, 50-68 (1992).
     

Related bibliography

  • K. Gopalakrishnan and G. Bodenhausen
    Cross polarization from spins I = 1/2 to spins S = 1 in nuclear magnetic resonance with magic angle sample spinning,
    J. Chem. Phys. 124, 194311/1-194311/14 (2006).
     
  • C. P. Grey, W. S. Veeman, and A. J. Vega
    Rotational echo 14N/13C/1H triple resonance solid-state nuclear magnetic resonance: a probe of 13C-14N internuclear distances,
    J. Chem. Phys. 98, 7711-7724 (1993).
     
 

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[Contact me] - Last updated December 15, 2012
Solid-state NMR bibliography for
Aluminum-27
Antimony-121/123
Arsenic-75
Barium-135/137
Beryllium-9
Bismuth-209
Boron-11
Bromine-79/81
Calcium-43
Cesium-133
Chlorine-35/37
Chromium-53
Cobalt-59
Copper-63/65
Deuterium-2
Gallium-69/71
Germanium-73
Gold-197
Hafnium-177/179
Indium-113/115
Iodine-127
Iridium-191/193
Krypton-83
Lanthanum-139
Lithium-7
Magnesium-25
Manganese-55
Mercury-201
Molybdenum-95/97
Neon-21
Nickel-61
Niobium-93
Nitrogen-14
Osmium-189
Oxygen-17
Palladium-105
Potassium-39/41
Rhenium-185/187
Rubidium-85/87
Ruthenium-99/101
Scandium-45
Sodium-23
Strontium-87
Sulfur-33
Tantalum-181
Titanium-47/49
Vanadium-51
Xenon-131
Zinc-67
Zirconium-91



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