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29Si MAS QCPMG echo train of zeolite LSX

Experiment performed with 4-mm diameter rotor spinning at 10 kHz.

Silicon-29 QCPMG echo train of LSX zeolite

29Si MAS QCPMG echo train of zeolite LSX


Acquisition parameters:

General  
PULPROG qcpmg.fau
TD 31288
NS 48
DS 0
SWH [Hz] 20000.00
AQ [s] 0.7822500
RG 128
DW [µs] 25.000
DE [µs] 6.50
const1 31287.650391
CONST11 0.0000000
D1 [s] 180.00000000
D3 [s] 0.00005000
D6 [s] 0.02000000
L22 19
P25 [µs] 0.00
rest [s] 0.00005873
Channel f1  
NUC1 29Si
P3 [µs] 6.35
P4 [µs] 12.70
PL1 [dB] 120
PL1W [W] 0.00000000
PL21 [dB] 6.00
PL21W [W] 130.48197937
PL22 [dB] 6.00
PL22W [W] 130.48197937
SFO1 [MHz] 99.3690980

29Si MAS QCPMG echo train of zeolite NaX

Experiment performed with 4-mm diameter rotor spinning at 10 kHz.

Silicon-29 QCPMG echo train of NaX zeolite

29Si MAS QCPMG echo train of NaX


Acquisition parameters:

General  
PULPROG qcpmg.fau
TD 4604
NS 336
DS 0
SWH [Hz] 20000.00
AQ [s] 0.1151500
RG 128
DW [µs] 25.000
DE [µs] 6.50
const1 4602.572266
CONST11 0.0000000
D1 [s] 180.00000000
D3 [s] 0.00005000
D6 [s] 0.00600000
L22 9
P25 [µs] 0.00
rest [s] 0.00008569
Channel f1  
NUC1 29Si
P3 [µs] 6.35
P4 [µs] 12.70
PL1 [dB] 120
PL1W [W] 0.00000000
PL21 [dB] 6.00
PL21W [W] 130.48197937
PL22 [dB] 6.00
PL22W [W] 130.48197937
SFO1 [MHz] 99.3690980

29Si MAS QCPMG echo train of zeolite NaY

Experiment performed with 4-mm diameter rotor spinning at 10 kHz.

Silicon-29 QCPMG echo train of NaY zeolite

29Si MAS QCPMG echo train of NaY


Acquisition parameters:

General  
PULPROG qcpmg.fau
TD 13468
NS 72
DS 0
SWH [Hz] 20000.00
AQ [s] 0.3367500
RG 128
DW [µs] 25.000
DE [µs] 6.50
const1 13466.829102
CONST11 0.0000000
D1 [s] 180.00000000
D3 [s] 0.00005000
D6 [s] 0.00400000
L22 41
P25 [µs] 0.00
rest [s] 0.00007929
Channel f1  
NUC1 29Si
P3 [µs] 6.35
P4 [µs] 12.70
PL1 [dB] 120
PL1W [W] 0.00000000
PL21 [dB] 6.00
PL21W [W] 130.48197937
PL22 [dB] 6.00
PL22W [W] 130.48197937
SFO1 [MHz] 99.3685010

29Si MAS QCPMG echo train of zeolite LZY64

Experiment performed with 4-mm diameter rotor spinning at 10 kHz.

Silicon-29 QCPMG echo train of LZY64 zeolite

29Si MAS QCPMG echo train of LZY64



29Si MAS QCPMG echo train of stabilized zeolite NH4Y, Si/Al = 6

Experiment performed with 4-mm diameter rotor spinning at 10 kHz.

Silicon-29 QCPMG echo train of stabilized NH4Y zeolite, Si/Al = 6

29Si MAS QCPMG echo train of stabilized zeolite NH4Y, Si/Al = 6


Acquisition parameters:

General  
PULPROG qcpmg.fau
TD 13468
NS 288
DS 0
SWH [Hz] 20000.00
AQ [s] 0.3367500
RG 128
DW [µs] 25.000
DE [µs] 6.50
const1 13466.829102
CONST11 0.0000000
D1 [s] 180.00000000
D3 [s] 0.00005000
D6 [s] 0.00400000
L22 41
P25 [µs] 0.00
rest [s] 0.00007929
Channel f1  
NUC1 29Si
P3 [µs] 6.35
P4 [µs] 12.70
PL1 [dB] 120
PL1W [W] 0.00000000
PL21 [dB] 6.00
PL21W [W] 130.48197937
PL22 [dB] 6.00
PL22W [W] 130.48197937
SFO1 [MHz] 99.3675560

29Si MAS QCPMG echo train of zeolite Beta

Experiment performed with 4-mm diameter rotor spinning at 12 kHz.

Silicon-29 QCPMG echo train of Beta zeolite

29Si MAS QCPMG echo train of zeolite Beta


Acquisition parameters:

General  
PULPROG qcpmg.fau
TD 12818
NS 240
DS 0
SWH [Hz] 20000.00
AQ [s] 0.3205000
RG 128
DW [µs] 25.000
DE [µs] 6.50
const1 12817.812500
CONST11 0.0000000
D1 [s] 180.00000000
D3 [s] 0.00005000
D6 [s] 0.00400000
L22 39
P25 [µs] 0.00
rest [s] 0.00005467
Channel f1  
NUC1 29Si
P3 [µs] 6.35
P4 [µs] 12.70
PL1 [dB] 120
PL1W [W] 0.00000000
PL21 [dB] 6.00
PL21W [W] 130.48197937
PL22 [dB] 6.00
PL22W [W] 130.48197937
SFO1 [MHz] 99.3669695

29Si MAS QCPMG echo train of zeolite Silicalite

Experiment performed with 4-mm diameter rotor spinning at 12 kHz.

Silicon-29 QCPMG echo train of Silicalite zeolite

29Si MAS QCPMG echo train of zeolite Silicalite


Acquisition parameters:

General  
PULPROG qcpmg.fau
TD 83188
NS 320
DS 0
SWH [Hz] 20000.00
AQ [s] 2.0797501
RG 128
DW [µs] 25.000
DE [µs] 6.50
const1 83186.828125
CONST11 0.0000000
D1 [s] 180.00000000
D3 [s] 0.00005000
D6 [s] 0.02500000
L22 41
P25 [µs] 0.00
rest [s] 0.00007936
Channel f1  
NUC1 29Si
P3 [µs] 6.35
P4 [µs] 12.70
PL1 [dB] 120
PL1W [W] 0.00000000
PL21 [dB] 6.00
PL21W [W] 130.48197937
PL22 [dB] 6.00
PL22W [W] 130.48197937
SFO1 [MHz] 99.3665330

 
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